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摘要: 采用固相反应法制备了正交单相PrBa2Cu3O7-δ样品.运用标准直流四引线法测量了该样品的电阻,发现它随温度的变化呈半导体行为.通过XPS测量表明,样品中明显合有Pr4+.最后从能带结构讨论了PtBa2Cu307-δ不超导的原因.
Abstract: Single phase samples of PrBa2Cu3O7-δ with orthorhombic structure were prepared by solid State reaction method. Resistance measurement was performed by a standard dc four-probe technique. It is found that the resistance exhibits semiconductor-like behavior. Results of XPS measurement indicate obviously the existence of Pr4+ in PrBa2Cu3O7-δ. Finally, the band structure was used to discuss the reasor why PrBa2Cu3O7-δ does not show superconductivity.