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中心挡板对扫描相干X射线衍射成像的影响

刘海岗 许子健 张祥志 郭智 邰仁忠

中心挡板对扫描相干X射线衍射成像的影响

刘海岗, 许子健, 张祥志, 郭智, 邰仁忠
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  • 本文采用重叠关联迭代引擎算法, 系统地模拟研究了扫描相干衍射成像中中心挡板导致的低频信号丢失对重建图像质量的影响. 结果表明, 扫描相干衍射成像对中心挡板的承受能力远大于平面波单次相干衍射成像, 且选择小尺寸入射探针和较高重叠度( 70%)可进一步降低中心丢失信号对扫描相干衍射成像的负面影响. 另外, 光斑扫描位置误差在重叠度较高时将超过中心挡板成为扫描相干衍射成像最主要的负面影响因素. 本文研究结果对扫描相干衍射成像实验中如何应用中心挡光板具有重要的指导意义, 将有助于进一步提高扫描相干衍射成像的分辨率.
    • 基金项目: 中国科学院知识创新工程重要方向性项目(批准号: KJCX2-YW-N38);上海市自然科学基金(批准号: 11ZR1445200);国家自然科学基金青年基金(批准号: 11005147)和中国科学院大科学装置开放研究项目;自组装技术与超高密度纳米阵列研究项目资助的课题.
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    [2]

    Miao J W, Charalambous P, Kirz J, Sayre D 1999 Nature 400 342

    [3]

    Miao J W Ishikawa T, Johnson B, Anderson E H, Lai B, Hodgson K O 2002 Phys. Rev. Lett. 89 088303

    [4]

    Shapiro D, Thibault P, Beetz T, Elser V, Howells M, Jacobsen C, Kirz J, Lima E, Miao H J, Neiman A M, Sayre D 2005 Proc. Natl. Acad. Sci. USA 102 15343

    [5]

    Schroer C G, Boye P, Feldkamp J M, Patommel J, Schropp A, Schwab A, Stephan S, Burghammer M, Schöder S, Riekel C 2008 Phys. Rev. Lett. 101 090801

    [6]

    Abbey B, Whitehead L W, Quiney H M, Vine D J, Cadenazzi G A, Henderson C A, Nugent K A, Balaur E, Putkunz C T, Peele A G, Williams G J, McNulty I 2011 Nature Photon. 5 420

    [7]

    Raines K S, Salha S, Sandberg R L, Jiang H D, Rodriguez J A, Fahimian B P, Kapteyn H C, Du J C, Miao J W 2010 Nature 463 214

    [8]

    Putkunz C T, Clark J N, Vine D J, Williams G J, Pfeifer M A, Balaur E, McNulty I, Nugent K A, Peele A G 2011 Phys. Rev. Lett. 106 013903

    [9]

    Dierolf M, Menzel A, Thibault P, Schneider P, Kewish C M, Wepf R, Bunk O, Pfeiffer F 2010 Nature 467 436

    [10]

    Beckers M, Senkbeil T, Gorniak T, Reese M, Giewekemeyer K, Gleber S C, Salditt T, Rosenhahn A 2011 Phys. Rev. Lett. 107 208101

    [11]

    Tripathi A, Mohanty J, Dietze S H, Shpyrko O G, Shipton E, Fullerton E E, Kim S S, McNulty I 2011 Proc. Natl. Acad. Sci. USA 108 13393

    [12]

    Nelson J, Huang X J, Steinbrener J, Shapiro D, Kirz J, Marchesini S, Neiman A M, Turner J J, Jacobsen C 2010 Proc. Natl. Acad. Sci. USA 107 7235

    [13]

    Jiang H D, Song C Y, Chen C C, Xu R, Raines K S, Rahimian B P, Lu C H, Lee T K, Nakashima A, Urano J, Ishikawa T, Tamanoi F, Miao J W 2010 Proc. Natl. Acad. Sci. USA 107 11234

    [14]

    Giewekemeyer K, Thibault P, Kalbfleisch S, Beerlink A, Kewish C M, Dierolf M, Pfeiffer F, Salditt T 2010 Proc. Natl. Acad. Sci. USA 107 529

    [15]

    Abbey B, Nugent K A, Williams G J, Clark J N, Peele A G, Pfeifer M A, Jonge M D, McNulty I 2008 Nature Phys. 4 394

    [16]

    Williams G J, Quiney H M, Dhal B B, Tran C Q, Nugent K A, Peele A G, Paterson D, Jonge M D 2006 Phys. Rev. Lett. 97 025506

    [17]

    Huang X J, Nelson J, Kirz J, Lima E, Marchesini S, Miao H J, Neiman A M, Shapiro D, Steinbrener J, Stewart A, Turner J J, Jacobsen C 2009 Phys. Rev. Lett. 103 198101

    [18]

    Whitehead L W, Williams G J, Quiney H M, Vine D J, Dilanian R A, Flewett S, Nugent K A 2009 Phys. Rev. Lett. 103 243902

    [19]

    Johnson I, Jefimovs K, Bunk O, David C, Dierolf M, Gray J, Renker D, Pfeiffer F 2008 Phys. Rev. Lett. 100 155503

    [20]

    Song C Y, Jiang H D, Mancuso A, Amirbekian B, Peng L, Sun R, Shah S S, Zhou Z H, Ishikawa T, Miao J W 2008 Phys. Rev. Lett. 101 158101

    [21]

    Jiang H D, Johnson D R, Song C Y, Amirbekian B, Kohmura Y, Nishino Y, Takahashi Y, Ishikawa T, Miao J W 2008 Phys. Rev. Lett. 100 038103

    [22]

    Song C Y, Bergstrom R, Johnson D R, Jiang H D, Paterson D, de Jonge M D, McNulty I, Lee J Y, Wang K, Miao J W 2008 Phys. Rev. Lett. 100 025504

    [23]

    Fan J D, Jiang H D 2012 Acta Phys. Sin. 61 218702 (in Chinese) [范家东, 江怀东 2012 物理学报 61 218702]

    [24]

    Huang W J, Zuo J M, Jiang B, Kwon K W, Shim M 2009 Nature Phys. 5 129

    [25]

    Scott M C Chen C C, Mecklenburg M, Zhu C, Xu R, Ercius P, Dahmen U, Regan B C, Miao J W 2012 Nature 483 444

    [26]

    Zuo J M, Vartanyants I, Gao M, Zhang R, Nagahara L A 2003 Science 300 1419

    [27]

    Seibert M M, Ekeberg T, Maia F, Svenda M, Andreasson J, Jönsson O, Odić D, Iwan B, Rocker A, Westphal D, Hantke M, DePonte D P, Barty A, Schulz J, Gumprecht L, Coppola N, Aquila A, Liang M N, White T A, Martin A, Caleman C, Stern S, Abergel C, Seltzer V, Claverie J, Bostedt C, Bozek J D, Boutet S, Miahnahri A A, Messerschmidt M, Krzywinski J, Williams G, Hodgson K O, Bogan M J, Hampton C Y, Sierra R G, Starodub D, Andersson I, Bajt S, Barthelmess M, Spence J C H, Fromme P, Weierstall U, Kirian R, Hunter M, Doak R B, Marchesini S, Hau-Riege S P, Frank M, Shoeman R L, Lomb L, Epp S W, Hartmann R, Rolles D, Rudenko A, Schmidt C, Foucar L, Kimmel N, Holl P, Rudek B, Erk B, Hömke A, Reich C, Pietschner D, Weidenspointner G, Strder L, Hauser G, Gorke H, Ullrich J, Schlichting I, Herrmann S, Schaller G, Schopper F, Soltau H, Khnel K U, Andritschke R, Schröter C D, Krasniqi F, Bott M, Schorb S, Rupp D, Adolph M, Gorkhover T, Hirsemann H, Potdevin G, Graafsma H, Nilsson B, Chapman H N, Hajdu J 2011 Nature 470 78

    [28]

    Chapman H N, Barty A, Bogan M J, Boutet S, Frank M, Hau-riege S P, Marchesini S, Woods B W, Bajt S, Benner W H, London R A, Plönjes E, Kuhlmann M, Treusch R, Dsterer S, Tschentscher T, Schneider J R, Spiller E, Möller T, Bostedt C, Hoener M, Shapiro D A, Hodgson K O, der Spoel D V, Burmeister F, Bergh M, Caleman C, Huldt G, Seibert M M, Maia F R N C, lee R W, Szöke A, Timneanu N, Hajdu J 2006 Nature Phys. 2 839

    [29]

    Sandberg R L, Song C Y, Wachulak P W, Raymondson D A, Paul A, Amirbekian B, Lee E, Sakdinawat A E, La-O-Vorakiat C, Marconi M C, Menoni C S, Murnane M M, Rocca J J, Kapteyn H C, Miao J W 2008 Proc. Natl. Acad. Sci. USA 105 24

    [30]

    Sandberg R L Paul A, Raymondson D A Hädrich S, Gaudiosi D M, Holtsnider J, Tobey R I, Cohen O, Murnane M M, Kapteyn H C, Song C, Miao J W, Liu Y W, Salmassi F 2007 Phys. Rev. Lett. 99 098103

    [31]

    Faulkner H M, Rodenburg J M 2004 Phys. Rev. Lett. 93 023903

    [32]

    Rodenburg J M, Faulkner H M 2004 Appl. Phys. Lett. 85 4795

    [33]

    Rodenburg J M, Hurst A C, Cullis A G 2007 Ultramicroscopy 107 227

    [34]

    Rodenburg J M, Hurst A C, Cullis A G, Dobson B R, Pfeiffer F, Bunk O, David C, Jefimovs K, Johnson I 2007 Phys. Rev. Lett. 98 034801

    [35]

    Thibault P, Dierolf M, Menzel A, Bunk O, David C, Pfeiffer F 2008 Science 321 379

    [36]

    Maiden A M, Rodenburg J M 2009 Ultramicroscopy 109 1256

    [37]

    Guizar-Sicairos M, Fienup J R 2008 Opt. Express 16 7264

    [38]

    Wilke R N, Priebe M, Bartels M, Giewekemeyer K, Diaz A, Karvinen P, Salditt T 2012 Opt. Express 20 19232

    [39]

    Takahashi Y, Suzuki A, Zettsu N, Kohmura Y, Senba Y, Ohashi H, Yamauchi K Ishikawa T 2011 Phys. Rev. B 83 214109

    [40]

    Miao J W, Nishino Y, Kohmura Y, Johnson B, Song C Y, Risbud S H, Ishikawa T 2005 Phys. Rev. Lett. 95 085503

    [41]

    He H, Marchesini S, Howells M, Weierstall U, Hembree G, Spence J C H 2003 Acta Crystallogr. Sect. A: Found. Crystallogr. 59 143

    [42]

    Zhou G Z, Tong Y J, Chen C, Ren Y Q, Wang Y D, Xiao T Q 2011 Acta Phys. Sin. 60 028701 (in Chinese) [周光照, 佟亚军, 陈灿, 任玉琦, 王玉丹, 肖体乔 2011 物理学报 60 028701]

    [43]

    Zhou G Z, Wang Y D, Ren Y Q, Chen C, Ye L L, Xiao T Q 2012 Acta Phys. Sin. 61 018701 (in Chinese) [周光照, 王玉丹, 任玉琦, 陈灿, 叶琳琳, 肖体乔 2012 物理学报 61 018701]

    [44]

    Miao J W, Sayre D, Chapman H N 1998 J. Opt. Soc. Am. A 15 1662

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  • 收稿日期:  2013-01-13
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中心挡板对扫描相干X射线衍射成像的影响

  • 1. 中国科学院上海应用物理研究所, 上海同步辐射光源, 上海 201800;
  • 2. 中国科学院大学, 北京 100049
    基金项目: 

    中国科学院知识创新工程重要方向性项目(批准号: KJCX2-YW-N38)

    上海市自然科学基金(批准号: 11ZR1445200)

    国家自然科学基金青年基金(批准号: 11005147)和中国科学院大科学装置开放研究项目

    自组装技术与超高密度纳米阵列研究项目资助的课题.

摘要: 本文采用重叠关联迭代引擎算法, 系统地模拟研究了扫描相干衍射成像中中心挡板导致的低频信号丢失对重建图像质量的影响. 结果表明, 扫描相干衍射成像对中心挡板的承受能力远大于平面波单次相干衍射成像, 且选择小尺寸入射探针和较高重叠度( 70%)可进一步降低中心丢失信号对扫描相干衍射成像的负面影响. 另外, 光斑扫描位置误差在重叠度较高时将超过中心挡板成为扫描相干衍射成像最主要的负面影响因素. 本文研究结果对扫描相干衍射成像实验中如何应用中心挡光板具有重要的指导意义, 将有助于进一步提高扫描相干衍射成像的分辨率.

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