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高分子薄膜表征技术

曾娴 杨朝晖 张晓华

高分子薄膜表征技术

曾娴, 杨朝晖, 张晓华
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  • 随着纳米技术在微电子、生物医药、能源等领域的快速发展,如何在纳米尺度构筑性能稳定、性质均一的多功能纳米器件已成为纳米科技领域最具有挑战性的前沿技术之一。 具有广泛应用前景的高分子薄膜的制备、性质以及应用研究一直以来都受到学术界与工业界的高度关注 对高分子薄膜的内部结构、表面形貌、机械性能、电化学性能等的检测一直是高分子领域的主要研究热点之一。 本文综述了高分子薄膜的测试方法,包括原子力显微镜、电子显微镜、X 光散射、中子散射、椭圆偏振光等表征技术.
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    Flier B M, Baier M C, Huber J, Mullen K, Mecking S, Zumbusch A, Woll D 2012 J. Am. Chem. Soc. 134 480

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    Yung P K, Mckenna G B, Simon S L 2006 J. Polym. Sci., Part B: Polym. Phys. 44 3518

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    Efremov M Y, Olson E A, Zhang M, Zhang Z, Allen L H 2003 Phys. Rev. Lett. 91 085703

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    Madkour S, Yin H, Fullbrandt M, Schonhals A 2015 Soft Matter 11 7942

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    Glor E C, Composto R J, Fakhraai Z 2015 Macromolecules 48 6682

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    Zhang X, Lacerda S H, Yager K G, Berry B C, Douglas J F, Jones R L, Karim A 2009 ACS Nano 3 2115

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    Drummy L F, Yang J, Martin D C 2004 Ultramicroscopy 99 247

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    Donald A M, He C B, Royall C P, Sferrazza M, Stelmashenko N A, Thiel B L 2000 Colloids Surf. A 174 37

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    Marjanski M, Srinivasarao M, Mirau P A 1998 Solid State Nucl. Magn. Reson. 12 113

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    Fukushima T, Kimura H, Shimahara Y, Kaji H 2011 Appl. Phys.Lett. 99 223301

  • [1]

    Alcoutlabi M, McKennad G B 2005 J. Phys.: Condens. Matter. 17 461

    [2]

    Kanaya T 2013 Glass Transition, Dynamics and Heterogeneity of Polymer Thin Films Advances in Polymer Science (Berlin: Springer) pp29-63

    [3]

    Keddie J L, Jones R A L, Cory R A 1994 Euro. Phys. Lett. 27 59

    [4]

    Forrest J A, Dalnoki-Veress K, Stevens J R, Dutcher J R 1996 Phys. Rev. Lett. 77 2002

    [5]

    Fukao K, Miyamoto Y 2000 Phys. Rev. E 61 1743

    [6]

    Ellison C J, Torkelson J M 2003 Nat. Mater. 2 695

    [7]

    Inoue R, Kanaya T, Nishida K, Tsukushi I, Shibata K 2005 Phys. Rev. Lett. 95 056102

    [8]

    Koh Y P, Mckenna G B, Simon S L 2006 Polym. Phys. 44 3518

    [9]

    Yang Z H, Fujii Y, Lee F K, Lam C H, Tsui O K C 2010 Science 328 1676

    [10]

    Napolitano S 2015 Non-equilibrium Phenomena in Confined Soft Matter (Switzerland: Springer) pp25-46

    [11]

    Jiang H, Dou N N, Fan G Q, Yang Z H, Zhang X H 2013 J. Chem. Phys. 139 124903

    [12]

    Shi H F, Jiang H, Fan G Q, Yang Z H, Zhang X H 2015 RSC Adv. 5 60015

    [13]

    Zhang X H, Yager K G, Fredin N J, Ro H W, Jones R L, Karim A, Douglas J F 2010 ACS Nano 4 3653

    [14]

    Tang C, Tracz A, Kruk M, Zhang R, Smilgies D M, Matyjaszewski K, Kowalewski T 2005 J. Am. Chem. Soc. 127 6918

    [15]

    Mller-Buschbaum P, Bauer E, Maurer E, Schlogl K, Roth S V, Gehrke R 2006 Appl. Phys. Lett. 88 083114

    [16]

    Zhang X, Yager K G, Douglas J F, Karim A 2014 Soft Matter 10 3656

    [17]

    Park S, Kwon K, Cho D, Lee B, Ree M, Chang T 2003 Macromolecules 36 4662

    [18]

    Meier R, Schindler M, Mller-Buschbaum P, Watts B 2011 Phys. Rev. B 84 174205

    [19]

    DeLongchamp D M, Kline R J, Fischer D A, Richter L J, Toney M F 2011 Adv. Mater. 23 319

    [20]

    Rogers J T, Schmidt K, Toney M F, Bazan G C, Kramer E 2012 J. Am. Chem. Soc. 134 2884

    [21]

    Kim B J, Miyamoto Y, Ma B, Frechet J M J 2009 Adv. Func. Mater. 19 2273

    [22]

    Smith K A, Lin Y H, Mok J W, Yager K G, Strzalka J, Nie W, Mohite A D, Verduzco R 2015 Macromolecules 48 8346

    [23]

    Reiter G 1994 Macromolecules 27 3046

    [24]

    Reiter G 1993 Europhys. Lett. 26 579

    [25]

    Schmitt J, Decher G, Dressick W J, Brandow S L, Geer R E, Shashidhar R, Calver J M 1997 Adv. Mater. 9 61

    [26]

    Swaraj S, Wang C, Yan HP, Watts B, Jan L N, McNeill C R, Ade H 2010 Nano Lett. 10 2863

    [27]

    Ma W, Tumbleston J R, Wang M, Gann E, Huang F, Ade H 2013 Adv. Energy Mater. 3 864

    [28]

    Tong M H, Cho S, Rogers J T, Schmidt K, Hsu B B Y, Moses D, Coffin R C, Kramer E J, Bazan G C, Heeger A J 2010 Adv. Funct. Mater. 20 3959

    [29]

    Lai L F, Yang H P, Wang L, Teh B K, Zhong J Q, Chou H, Chen L W, Chen W, Shen Z X, Ruoff R S 2012 ACS Nano 6 5941

    [30]

    Gurau M C, Delongchamp D M, Vogel B M, Lin E K, Fischer D A, Sambasivan S, Richter L J 2007 Langmuir 2 834

    [31]

    Morin C, Ikeura-Sekiguchi H, Tyliszczak T, Cornelius R, Brash J L, Hitchcock A P, Scholl A, Nolting F, Appel G, Winesett 2001 J. Electron Spectrosc. Relat. Phenom. 121 203

    [32]

    Zhang X H, Berry B C, Yager K G, Kim S, Jones R L, Satija S, Pickel D L, Douglas J F, Karim A 2008 ACS Nano 2 2331

    [33]

    Zhang X H, Douglas J F, Satija S, Karim A 2015 RSC Adv. 5 32307

    [34]

    Schmidt-Rohr K, Chen Q 2008 Nat. Mater. 7 75

    [35]

    Jones R L, Kumar S K, Ho D L, Briber R M, Russell T P 1999 Nature 400 146

    [36]

    Muller-Buschbaum P, Gutmann J S, Cubitt R, Petry W 2004 Phys. B 350 207

    [37]

    Tanaka M, Sackmann E 2005 Nature 437 656

    [38]

    Parnell A J, Dunbar A D F, Pearson A J, Staniec P A, Dennison A J C, Hamamatsu H, Skoda M W A, Lidzey D G, Jones R A L 2010 Adv. Mater. 22 2444

    [39]

    Kajiyama T, Tanaka K, Satomi N, Takahara A 1998 Macromolecules 31 5150

    [40]

    Hammerschmidt J A, Gladfelter W L, Haugstad G 1999 Macromolecules 32 3360

    [41]

    Tsui O K C, Wang X P, Ho J Y L, Ng T K, Xiao X 2000 Macromolecules 33 4198

    [42]

    Fryer D S, Peters R D, Kim E J, Tomaszewski J E, de Pablo J J, Nealey P F, White C C, Wu W L 2001 Macromolecules 34 5627

    [43]

    Fryer D S, Nealey P F, de Pablo J J 2000 Macromolecules 33 6439

    [44]

    Kawana S, Jones R A L 2001 Phys. Rev. E 63 021501

    [45]

    Mattsson J, Forrest J A, Borjesson L 2000 Phys. Rev. E 62 5187

    [46]

    Cheng W, Sainidou R, Burgardt P, Stefanou N, Kiyanova A, Efremov M, Fytas G, Nealey P F 2007 Macromolecules 40 7283

    [47]

    Hartschuh R, Ding Y, Roh J H, Kisliuk A, Sokolov A P, Soles C L, Jones R L, Hu T J, Wu W L, Mahorowala A P 2004 J. Polym. Sci., Part B: Polym. Phys. 42 1106

    [48]

    Kwak G, Fukao S, Fujiki M, Sakaguchi T, Masuda T 2006 Chem. Mater. 18 2081

    [49]

    Anastasiadis S H, Karatasos K, Vlachos G, Manias E, Giannelis E P 2000 Phys. Rev. Lett. 84 915

    [50]

    Rajendran S, Sivakumar M, Subadevi R 2004 Mater. Lett. 58 641

    [51]

    Tress M, Erber M, Mapesa E U, Huth H, Muller J, Serghei A, Schick C, Eichhorn K J, Volt B, Kremer F 2010 Macromolecules 43 9937

    [52]

    Flier B M, Baier M C, Huber J, Mullen K, Mecking S, Zumbusch A, Woll D 2012 J. Am. Chem. Soc. 134 480

    [53]

    Yung P K, Mckenna G B, Simon S L 2006 J. Polym. Sci., Part B: Polym. Phys. 44 3518

    [54]

    Efremov M Y, Olson E A, Zhang M, Zhang Z, Allen L H 2003 Phys. Rev. Lett. 91 085703

    [55]

    Madkour S, Yin H, Fullbrandt M, Schonhals A 2015 Soft Matter 11 7942

    [56]

    Glor E C, Composto R J, Fakhraai Z 2015 Macromolecules 48 6682

    [57]

    Zhang X, Lacerda S H, Yager K G, Berry B C, Douglas J F, Jones R L, Karim A 2009 ACS Nano 3 2115

    [58]

    Jinnai H, Kajihara T, Watashiba H, Nishikawa Y, Spontak R J 2001 Phys. Rev. E 64 010803

    [59]

    Park H W, Jung J, Chang T, Matsunaga K, Jinnai H 2009 J. Am. Chem. Soc. 131 46

    [60]

    Niihara K, Sugimori H, Matsuwaki U, Hirato F, Morita H, Doi M, Masunaga H, Sasaki S, Jinnai H 2008 Macromolecules 41 9318

    [61]

    Brinkmann M, Rannou P 2009 Macromolecules 42 1125

    [62]

    Salammal S T, Mikayelyan E, Grigorian S, Pietsch U, Koenen N, Scherf U 2012 Macromolecules 45 5575

    [63]

    Drummy L F, Yang J, Martin D C 2004 Ultramicroscopy 99 247

    [64]

    Donald A M, He C B, Royall C P, Sferrazza M, Stelmashenko N A, Thiel B L 2000 Colloids Surf. A 174 37

    [65]

    Marjanski M, Srinivasarao M, Mirau P A 1998 Solid State Nucl. Magn. Reson. 12 113

    [66]

    Fukushima T, Kimura H, Shimahara Y, Kaji H 2011 Appl. Phys.Lett. 99 223301

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出版历程
  • 收稿日期:  2016-05-20
  • 修回日期:  2016-07-06
  • 刊出日期:  2016-09-05

高分子薄膜表征技术

    基金项目: 

    国家自然科学基金(批准号:21274103,21204059)和2013年江苏省创新团队计划资助的课题.

摘要: 随着纳米技术在微电子、生物医药、能源等领域的快速发展,如何在纳米尺度构筑性能稳定、性质均一的多功能纳米器件已成为纳米科技领域最具有挑战性的前沿技术之一。 具有广泛应用前景的高分子薄膜的制备、性质以及应用研究一直以来都受到学术界与工业界的高度关注 对高分子薄膜的内部结构、表面形貌、机械性能、电化学性能等的检测一直是高分子领域的主要研究热点之一。 本文综述了高分子薄膜的测试方法,包括原子力显微镜、电子显微镜、X 光散射、中子散射、椭圆偏振光等表征技术.

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