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Preparation of ZrO2:Eu3+-Bi3+ phosphor and Bi3+ sensitizing characteristic emission of Eu3+ ions

Sang Shi-Jing Lü Shu-Chen Qu Xiu-Rong Yang Xiao-Xu Zhang Li-Li

Preparation of ZrO2:Eu3+-Bi3+ phosphor and Bi3+ sensitizing characteristic emission of Eu3+ ions

Sang Shi-Jing, Lü Shu-Chen, Qu Xiu-Rong, Yang Xiao-Xu, Zhang Li-Li
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  • Eu3+ and Bi3+ codoped ZrO2 nanocrystalline powders are prepared by chemical co-precipitation method. The room temperature characteristic emission of Eu3+ can be observed from each sample. We determine the crystal structures and luminescent properties of the samples. It is shown that the crystal phase of nanocrystalline ZrO2:Eu3+-Bi3+ powder calcined at 600 ℃ is tetragonal, and it turns into the mixture of tetragonal and monoclinic phase as temperature rises to 800, 950, and 1100 ℃. It is obvious that characteristic emission intensity of Eu3+ in the tetragonal phase is greater than in the mixed phase. Bi3+ can sensitize the room temperature characteristic emission of Eu3+ in nanocrystalline ZrO2.
    • Funds: Project supported by the Research Foundation of Education Bureau of Heilongjiang Province, China (Grant No. 12511z013).
    [1]

    Gouveia-Neto A S, Silva A F, Bueno L A, Costa E B 2012 J. Lumin. 132 299

    [2]

    Chang Y S, Shi Z R, Tsai Y Y, Wu S, Chen H L 2011 Opt. Mater. 33 375

    [3]

    Ding Y C, Zhao G J, Nakai Y, Tsuboi T 2011 J. Alloys Compd. 509 7488

    [4]

    Zhang J C, Qin Q S, Yu M H 2012 J. Lumin. 132 23

    [5]

    Tanabe S, Hayashi H, Hanada T, Onodera N 2002 Opt. Mater. 19 343

    [6]

    Li X M, Lü S C, Liu J X 2007 Chin. J. Lumin. 28 378 (in Chinese) [李秀明, 吕树臣, 刘金霞 2007 发光学报 28 378]

    [7]

    Liu J X, Lü S C, Li X M 2004 J.Chin. RE Soc. 22 867 (in Chinese) [刘金霞, 吕树臣, 李秀明 2004 中国稀土学报 22 867]

    [8]

    Li X M, Lü S C, Liu J X 2005 Chin. J. Lumin. 26 220 (in Chinese) [李秀明, 吕树臣, 刘金霞 2005 发光学报 26 220]

    [9]

    Zhou W, Lü S C 2008 Chin. J. Lumin. 29 176 (in Chinese) [周巍, 吕树臣2008 发光学报 29 176]

    [10]

    Liu J X, Lü S C 2006 J. Synth. Cryst. 35 1129 (in Chinese) [刘金霞, 吕树臣 2006 人工晶体学报 35 1129]

    [11]

    Tan X X, Lü S C 2010 Acta Photonica Sin. 39 1169 (in Chinese) [谭鑫鑫, 吕树臣 2010 光子学报 39 1169]

    [12]

    Liu J X, Lü S C, Li X M 2006 Spectrosc. Spectral Anal. 26 605 (in Chinese) [刘金霞, 吕树臣, 李秀明 2006 光谱学与光谱分析 26 605]

    [13]

    Lü J T, Wang K J, Liu J S, Zhang Q Q, Zhu Q H, Zeng X M, Yao J Q 2011 Acta Opt. Sin. 31 1116001 (in Chinese) [吕健滔, 王可嘉, 刘劲松, 张清泉, 朱启华, 曾小明, 姚建铨 2011光学学报 31 1116001]

    [14]

    Wang Z L, Wang Y H, Zhang J C 2008 Chem. Res. Chin. Univ. 24 679

    [15]

    Zhong R X, Zhang J H, Li M Y, Wang X Q 2012 Acta Phys. Sin. 61 117801 (in Chinese) [钟瑞霞, 张家骅, 李明亚, 王晓强 2012 物理学报 61 117801]

    [16]

    Xu W, Li C R, Chen B J, Feng Z Q 2010 Acta Phys. Sin. 59 1328 (in Chinese) [徐伟, 李成仁, 陈宝玖, 冯志 2010 物理学报 59 1328]

    [17]

    Zhang Q H, Wang J, Ni H Y, Wang L L 2012 Rare Met. 31 35

  • [1]

    Gouveia-Neto A S, Silva A F, Bueno L A, Costa E B 2012 J. Lumin. 132 299

    [2]

    Chang Y S, Shi Z R, Tsai Y Y, Wu S, Chen H L 2011 Opt. Mater. 33 375

    [3]

    Ding Y C, Zhao G J, Nakai Y, Tsuboi T 2011 J. Alloys Compd. 509 7488

    [4]

    Zhang J C, Qin Q S, Yu M H 2012 J. Lumin. 132 23

    [5]

    Tanabe S, Hayashi H, Hanada T, Onodera N 2002 Opt. Mater. 19 343

    [6]

    Li X M, Lü S C, Liu J X 2007 Chin. J. Lumin. 28 378 (in Chinese) [李秀明, 吕树臣, 刘金霞 2007 发光学报 28 378]

    [7]

    Liu J X, Lü S C, Li X M 2004 J.Chin. RE Soc. 22 867 (in Chinese) [刘金霞, 吕树臣, 李秀明 2004 中国稀土学报 22 867]

    [8]

    Li X M, Lü S C, Liu J X 2005 Chin. J. Lumin. 26 220 (in Chinese) [李秀明, 吕树臣, 刘金霞 2005 发光学报 26 220]

    [9]

    Zhou W, Lü S C 2008 Chin. J. Lumin. 29 176 (in Chinese) [周巍, 吕树臣2008 发光学报 29 176]

    [10]

    Liu J X, Lü S C 2006 J. Synth. Cryst. 35 1129 (in Chinese) [刘金霞, 吕树臣 2006 人工晶体学报 35 1129]

    [11]

    Tan X X, Lü S C 2010 Acta Photonica Sin. 39 1169 (in Chinese) [谭鑫鑫, 吕树臣 2010 光子学报 39 1169]

    [12]

    Liu J X, Lü S C, Li X M 2006 Spectrosc. Spectral Anal. 26 605 (in Chinese) [刘金霞, 吕树臣, 李秀明 2006 光谱学与光谱分析 26 605]

    [13]

    Lü J T, Wang K J, Liu J S, Zhang Q Q, Zhu Q H, Zeng X M, Yao J Q 2011 Acta Opt. Sin. 31 1116001 (in Chinese) [吕健滔, 王可嘉, 刘劲松, 张清泉, 朱启华, 曾小明, 姚建铨 2011光学学报 31 1116001]

    [14]

    Wang Z L, Wang Y H, Zhang J C 2008 Chem. Res. Chin. Univ. 24 679

    [15]

    Zhong R X, Zhang J H, Li M Y, Wang X Q 2012 Acta Phys. Sin. 61 117801 (in Chinese) [钟瑞霞, 张家骅, 李明亚, 王晓强 2012 物理学报 61 117801]

    [16]

    Xu W, Li C R, Chen B J, Feng Z Q 2010 Acta Phys. Sin. 59 1328 (in Chinese) [徐伟, 李成仁, 陈宝玖, 冯志 2010 物理学报 59 1328]

    [17]

    Zhang Q H, Wang J, Ni H Y, Wang L L 2012 Rare Met. 31 35

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  • Received Date:  06 April 2012
  • Accepted Date:  13 June 2012
  • Published Online:  20 November 2012

Preparation of ZrO2:Eu3+-Bi3+ phosphor and Bi3+ sensitizing characteristic emission of Eu3+ ions

  • 1. Key Laboratory of Photoelectric Bandgap Materials, Ministry of Education, Harbin Normal University, Harbin 150025 , China
Fund Project:  Project supported by the Research Foundation of Education Bureau of Heilongjiang Province, China (Grant No. 12511z013).

Abstract: Eu3+ and Bi3+ codoped ZrO2 nanocrystalline powders are prepared by chemical co-precipitation method. The room temperature characteristic emission of Eu3+ can be observed from each sample. We determine the crystal structures and luminescent properties of the samples. It is shown that the crystal phase of nanocrystalline ZrO2:Eu3+-Bi3+ powder calcined at 600 ℃ is tetragonal, and it turns into the mixture of tetragonal and monoclinic phase as temperature rises to 800, 950, and 1100 ℃. It is obvious that characteristic emission intensity of Eu3+ in the tetragonal phase is greater than in the mixed phase. Bi3+ can sensitize the room temperature characteristic emission of Eu3+ in nanocrystalline ZrO2.

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