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大角度会聚束电子衍射的新方法

冯国光

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大角度会聚束电子衍射的新方法

冯国光

A NEW METHOD FOR OBTAINING LARGE-ANGLE CONVERGENT-BEAM ELECTRON DIFFRACTION

FENG GUO-GUANG
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  • 会聚束电子衍射是测定晶体点群、空间群的有效方法。要清楚地判断会聚束电子衍射图样的对称性,电子束的会聚角要大,但衍射盘不能重叠。本文提出了一种新方法来获得不重叠的大角度会聚束电子衍射。新方法是使电子束离焦,固定样品,从而保留了样品的同心倾动位置,作大角度倾动时不会失去原来感兴趣的区域。新方法在原理上和田中等人提出的方法相同,但优越性更大。同时也研究了大束斑(≥2μm)大角度会聚束电子衍射。
    The symmetry of CBBD patterns provides a powerful means for determ'ning the crystal point groups and space groups. To obtain a useful CBED pattern, the angle of convergence of the electron beam must be large enough, but the diffraction discs must not overlap. A new method for obtaining non-overlapping large-angle CBED is proposed here. The principle of this method is equivalent to that proposed by Tanaka et al. Instead of shifting the specimen, the electron beam is defocused, thus retaining the eccentric height of the specimen. Hence the area of interest will not be lost when the specimen is tilted. Large-angle CBED patterns generated by a large electron probe (>2μm) may besdistorted, but they are useful.
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出版历程
  • 收稿日期:  1983-11-29
  • 刊出日期:  2005-03-25

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