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插入二氧化铈薄膜提高MOD-YBa2Cu3O7-x厚膜超导性能的研究

丁发柱 古宏伟 王洪艳 屈飞 商红静 张慧亮 董泽斌 张贺 周微微

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插入二氧化铈薄膜提高MOD-YBa2Cu3O7-x厚膜超导性能的研究

丁发柱, 古宏伟, 王洪艳, 屈飞, 商红静, 张慧亮, 董泽斌, 张贺, 周微微

Enhanced superconducting properties in MOD-YBCO thick films with CeO2 interlayer

Ding Fa-Zhu, Gu Hong-Wei, Wang Hong-Yan, Qu Fei, Shang Hong-Jing, Zhang Hui-Liang, Dong Ze-Bin, Zhang He, Zhou Wei-Wei
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  • YBa2Cu3O7-x(YBCO)膜存在厚度效应: 随着厚度增加, YBCO薄膜的临界电流密度下降, 尤其是YBCO薄膜的厚度超过1 m时, 它的临界电流密度急剧下降. 本文在YBCO薄膜之间引入极薄的二氧化铈(CeO2)薄膜, 成功制备出结构为YBCO/YBCO/CeO2/YBCO的超导厚膜. 所制备的厚度为2 m的YBCO膜临界电流密度为1.36 MA/cm2 (77 K, 自场), 其性能比相同厚度的纯YBCO膜有了较大幅度的提升. 研究表明CeO2薄膜起到了传递织构、松弛应力的作用.
    In YBa2Cu3O7-x (YBCO) film there exists thickness effect: the critical current density of YBCO film drops precipitously as the coating thickness increases, especially in the case that the thickness of YBCO film exceeds 1 m. In this paper, we introduce very thin layers of CeO2 into YBCO layers and successfully fabricate the structure of YBCO/YBCO/CeO2/YBCO superconducting thick film. Firstly, YBCO films with two layers are fabricated on a LaAlO3 substrate by a multiple coatings process using a trifluoroacetate metal organic deposition method. Secondly, CeO2 thin films are deposited on YBCO films by RF-sputtering. Finally, we prepare the third YBCO film on CeO2interlayer. No cracks are observed in scanning electron microscopy images of these films; further, the majority of the grains in the films are well-textured and c-axis oriented. The full-width-half-maximum of the out-of-plane texture is measured to be 1.395 for the multilayer YBCO film at a thickness of 2 m Using this multilayer technology, we achieve Jc values of up to 1.36 MA/cm2 (77 K, self-field) in films as thick as 2 m, for an extrapolated critical current of 272 A/cm. We attribute the enhanced performance of the thick YBCO film to the CeO2 interlayer which playsan important role in transmission texture and stress relaxation.
      通信作者: 古宏伟, guhw@mail.iee.ac.cn
    • 基金项目: 国家高技术研究发展计划(批准号: 2014AA032702)、国家自然科学基金(批准号: 51577180, 51272250)和北京市自然科学基金面上项目(批准号: 2152035)资助的课题.
      Corresponding author: Gu Hong-Wei, guhw@mail.iee.ac.cn
    • Funds: Project supported by the National Higy Technology Research and Development Program of China (Grant No. 2014AA032702), the National Nature Science Foundation of China (Grant Nos. 51577180, 51272250) and the Beijing Natural Science Foundation, China (Grant No. 2152035).
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    [2]

    Moon S H, Su Nam 2013 Developed New Process Named RCE-DR: The Practical Highest Throughput Process. European Conference on Applied Superconductivity Genova, Italy, September 15-19, 2013

    [3]

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    [4]

    Malozemoff A P 2015 Progress in American Superconductor's HTS Wire and Optimization for Fault Current Limiting Systems, 28th International Symposium on Superconductivity Tokyo, Japan, November 16-18, 2015

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    Ibi A, Iwai H, Takahashi K, Muroga T, Miyata S, Watanabe T, Yamada Y, Shiohara Y 2005 Physica C: Superconductivity 426-431 910

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    Li X, Rupich M W, Kodenkandath T, Huang Y 2007 IEEE Trans. Appl. Supercond. 17 3553

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    Teranishi R, Matsuda J, Nakaoka K, Fuji H, Aoki Y, Kitoh Y, Nomoto S, Yamada Y, Yajima A, Izumi T, Shiohara Y 2005 Physica C: Superconductivity 426-431 959

    [8]

    Matsui H, Tsukada K, Tsuchiya T, Sohma M, Yamaguchi I, Manabe T, Kumagai T 2011 IEEE Trans. Appl. Supercond. 21 2933

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    [13]

    Takahashi K, Kobayashi H, Yamada Y, Ibi A, Fukushima H, Konishi M, Miyata S, Shiohara Y, Kato T, Hirayama T 2006 Supercond. Sci. Technol. 19 924

    [14]

    Foltyn S R, Jia Q X, Arendt P N, Kinder L, Fan Y, Smith J F 1999 Appl. Phys. Lett. 75 3692

    [15]

    Pahlke P, Hering M, Sieger M, Lao M, Eisterer M, Usoskin A, Strmer J, Holzapfel B, Schultz L, Hhne R 2015 IEEE Trans. Appl. Supercond. 25 3

    [16]

    Ding F Z, Gu H W, Wang H Y, Zhang H L, Zhang T, Qu F, Dong Z B, Zhou W W 2015 Chin. Phys. B 24 057401

    [17]

    Foltyn S R, Wang H, Civale L, Jia Q X, Arendt P N, Maiorov B, Li Y, Maley M P, MacManus-Driscoll J L 2005 Appl. Phys. Lett. 87 162505

    [18]

    Feldmann D M, Holesinger T G, Maiorov B, Zhou H, Foltyn S R, Coulter J Y, Apodoca I 2010 Supercond. Sci. Technol. 23 115016

    [19]

    Sarkara A, Danga V S, Mikheenko P, Awang Kechik M M, Abell J S, Crisan A 2010 Thin Solid Film 519 876

    [20]

    Teranishi R, Matsuda J, Nakaoka K, Fuji H, Aoki Y, Kitoh Y, Izumi T, Yamada Y, Shiohara Y 2005 IEEE Trans. Appl. Supercond. 15 2663

    [21]

    Matsui H, Tsukada K, Tsuchiya T, Sohma M, Yamaguchi I, Manabe T, Kumagai T 2011 IEEE Trans. Appl. Supercond. 21 2933

    [22]

    Zhu Y B, Zhou Y L, Wang S F, Liu Z, Zhang Q, Chen Z H, L H B, Yang G Z 2004 Chin. Phys. B 13 238

    [23]

    Ding F Z, L X D, Gu H W, Li T, Cao J L 2009 Chin. Phys. B 18 1631

    [24]

    Ghalsasi S, Zhou Y X, Chen J, L B, Salama K 2008 Supercond. Sci. Technol. 21 045015

    [25]

    Shu G Q, Li M J, Boubeche M, Liu Z Y, Bai C Y, Cai C B 2014 IEEE Trans. Appl. Supercond. 24 5

  • [1]

    Fukushima T, Nakasaki R, Zhang Y, Brownsey P, Sundaram A, Kasahara M, Kuraseko H, Hazelton D, Sakamoto H 2015 Performance and Reliability of 2G-HTS Wires for High-Field Magnet Applications, 28th International Symposium on Superconductivity Tokyo, Japan, November 16-18, 2015

    [2]

    Moon S H, Su Nam 2013 Developed New Process Named RCE-DR: The Practical Highest Throughput Process. European Conference on Applied Superconductivity Genova, Italy, September 15-19, 2013

    [3]

    Iijima Y, Adachi Y, Igarashi M, Kakimoto K, Fujita S, Daibo M, Ohsugi M, Takemoto T, Nakamura N, Kurihara C, Machida K, Hanyu S Kikutake R, Nagata M, Tatano F, Itoh M 2014 Development for Mass Production of Homogeneous RE123 Coated Conductors by Hot-Wall PLD Process on IBAD Template Technique, Applied Superconductivity Conference Charlotte NC, USA, August 10-15, 2014

    [4]

    Malozemoff A P 2015 Progress in American Superconductor's HTS Wire and Optimization for Fault Current Limiting Systems, 28th International Symposium on Superconductivity Tokyo, Japan, November 16-18, 2015

    [5]

    Ibi A, Iwai H, Takahashi K, Muroga T, Miyata S, Watanabe T, Yamada Y, Shiohara Y 2005 Physica C: Superconductivity 426-431 910

    [6]

    Li X, Rupich M W, Kodenkandath T, Huang Y 2007 IEEE Trans. Appl. Supercond. 17 3553

    [7]

    Teranishi R, Matsuda J, Nakaoka K, Fuji H, Aoki Y, Kitoh Y, Nomoto S, Yamada Y, Yajima A, Izumi T, Shiohara Y 2005 Physica C: Superconductivity 426-431 959

    [8]

    Matsui H, Tsukada K, Tsuchiya T, Sohma M, Yamaguchi I, Manabe T, Kumagai T 2011 IEEE Trans. Appl. Supercond. 21 2933

    [9]

    Jia Q X, Foltyn S R, Arendt P N, Smith J F 2002 Appl. Phys. Lett. 80 1601

    [10]

    Suenaga M, Li Q, Ye Z, Iwakuma M, Toyota K, Funaki F, Foltyn S R, Wang H, Clem J R 2004 J. Appl. Phys. 95 208

    [11]

    Feldmann D M, Holesinger T G, Maiorov B, Zhou H, Foltyn S R, Coulter J Y, Apodoca I 2010 Supercond. Sci. Technol. 23 115016

    [12]

    Rupich M W, Li X P, Sathyamurthy S, Thieme C L H, DeMoranville K, Gannon J, Fleshler S 2013 IEEE Trans. Appl. Supercond. 23 6601205

    [13]

    Takahashi K, Kobayashi H, Yamada Y, Ibi A, Fukushima H, Konishi M, Miyata S, Shiohara Y, Kato T, Hirayama T 2006 Supercond. Sci. Technol. 19 924

    [14]

    Foltyn S R, Jia Q X, Arendt P N, Kinder L, Fan Y, Smith J F 1999 Appl. Phys. Lett. 75 3692

    [15]

    Pahlke P, Hering M, Sieger M, Lao M, Eisterer M, Usoskin A, Strmer J, Holzapfel B, Schultz L, Hhne R 2015 IEEE Trans. Appl. Supercond. 25 3

    [16]

    Ding F Z, Gu H W, Wang H Y, Zhang H L, Zhang T, Qu F, Dong Z B, Zhou W W 2015 Chin. Phys. B 24 057401

    [17]

    Foltyn S R, Wang H, Civale L, Jia Q X, Arendt P N, Maiorov B, Li Y, Maley M P, MacManus-Driscoll J L 2005 Appl. Phys. Lett. 87 162505

    [18]

    Feldmann D M, Holesinger T G, Maiorov B, Zhou H, Foltyn S R, Coulter J Y, Apodoca I 2010 Supercond. Sci. Technol. 23 115016

    [19]

    Sarkara A, Danga V S, Mikheenko P, Awang Kechik M M, Abell J S, Crisan A 2010 Thin Solid Film 519 876

    [20]

    Teranishi R, Matsuda J, Nakaoka K, Fuji H, Aoki Y, Kitoh Y, Izumi T, Yamada Y, Shiohara Y 2005 IEEE Trans. Appl. Supercond. 15 2663

    [21]

    Matsui H, Tsukada K, Tsuchiya T, Sohma M, Yamaguchi I, Manabe T, Kumagai T 2011 IEEE Trans. Appl. Supercond. 21 2933

    [22]

    Zhu Y B, Zhou Y L, Wang S F, Liu Z, Zhang Q, Chen Z H, L H B, Yang G Z 2004 Chin. Phys. B 13 238

    [23]

    Ding F Z, L X D, Gu H W, Li T, Cao J L 2009 Chin. Phys. B 18 1631

    [24]

    Ghalsasi S, Zhou Y X, Chen J, L B, Salama K 2008 Supercond. Sci. Technol. 21 045015

    [25]

    Shu G Q, Li M J, Boubeche M, Liu Z Y, Bai C Y, Cai C B 2014 IEEE Trans. Appl. Supercond. 24 5

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  • 收稿日期:  2016-01-11
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