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Top seeded infiltration and growth method (TSIG) is improved by adopting a new liquid source and novel configuration. And single-domain Gd-Ba-Cu-O (GdBCO) bulk superconductors are successfully prepared using the improved method. Experimental observations on the morphology and the microstructure show that the samples exhibit good texture and homogeneous distribution of fine Gd2BaCuO5 (Gd-211) inclusions. Superconductive measurements reveal that the sample exhibits high superconducting transition temperature, self-field critical current density, and strong levitation force. In addition, the improved method can be used to simplify the process flow, shorten the experimental cycle, and hance the stability of the process, thus reducing the experimental difficulties. The results lay a good foundation for the batch production of large single domain bulks.
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Keywords:
- GdBCO /
- infiltration and growth /
- liquid source /
- configuration
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[2] Feng Y, Zhou L, Yang W M, Zhang C P, Wang J R, Yu Z M, Wu X Z 2000 Acta Phys. Sin. 49 146 (in Chinese) [冯 勇、周 廉、杨万民、张翠萍、汪京荣、于泽铭、吴晓祖 2000 物理学报 49 146]
[3] Cai Y Q, Yao X, Li G 2006 Acta Phys. Sin. 55 844 (in Chinese) [蔡衍卿、姚 忻、李 刚 2006 物理学报 55 844]
[4] Zhang Y L, Yao X, Zhang H, Jin Y P 2005 Acta Phys. Sin. 54 3380 (in Chinese) [张玉龙、姚 忻、张 宏、金燕苹 2005 物理学报 54 3380]
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[7] Ding F Z, Lü X D, Gu H W, Li T, Cao J L 2009 Chin. Phys. B 18 1631
[8] Shen C X, Shen X L, Lu W, Dong X L, Li Z C, Xiong J W, Zhou F 2008 Chin. Phys. B 17 1425
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[11] Muralidhar M, Sakai N, Chikumoto N, Jirsa M, Machi T, Nishiyama M, Wu Y, Murakami M 2002 Phys. Rev. Lett. 89 237001
[12] Shen X L, Li Z C, Shen C X, Lu W, Dong X L, Zhou F, Zhao Z X 2009 Chin. Phys. B 18 2893
[13] Gawalek W, Habisreuther T, Zeisberger M, Litzkendorf D, Surzhenko O, Kracunovska S, Prikhna T A, Oswald B, Kovalev L K, Canders W 2004 Supercond. Sci. Technol. 17 1185
[14] Werfel F N, Floegel-Delor U, Rothfeld R, Goebel B, Wippich D, Riedel T 2005 Supercond. Sci. Technol. 18 S19
[15] Oswald B, Best K J, Setzer M, Soll M, Gawalek W, Gutt A, Kovalev L, Krabbes G, Fisher L, Freyhardt H C 2005 Supercond. Sci. Technol. 18 S24
[16] Dai J Q, Zhao Z X, Xiong J W 2003 Supercond. Sci. Technol. 16 815
[17] Babu N H, Iida K, Shi Y, Cardwell D A 2005 Appl. Phys. Lett. 87 202506
[18] Iida K, Babu N H, Shi Y, Cardwell D A 2005 Supercond. Sci. Technol. 18 1421
[19] Iida K, Babu N H, Shi Y, Cardwell D A 2006 Supercond. Sci. Technol. 19 S478
[20] Meslin S, Iida K, Babu N H, Cardwell D A, Noudem J G 2006 Supercond. Sci. Technol. 19 711
[21] Noudem J G, Meslin S, Horvath D, Harnois C, Chateigner D, Ouladdiaf B, Eve S, Gomina M, Chaud X, Murakami M 2007 J. Am. Ceram. Soc. 90 2784
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[23] Varanasi C, Mcginn P J, Blackstead H A, Pullinga D B 1995 Appl. Phys. Lett. 67 1004
[24] Feng Y, Zhou L, Wen J G, Koshizuka N, Sulpice A, Tholence J L, Vallier J C, Monceau P 1998 Physica C 297 75
[25] Zheng H, Jiang M, Huang Y, Veal B W, Claus H 1998 Physica C 307 284
[26] Nariki S, Sakai N, Murakami M, Hirabayashi I 2004 Physica C 412-414 557
[27] Iida K, Babu N H, Withnell T D, Shi Y, Haindl S, Weber H W, Cardwell D A 2006 Physica C 445-448 277
[28] Babu N H, Iida K, Shi Y, Cardwell D A 2006 Physica C 445-448 286
[29] Li G Z, Yang W M, Tang Y L, Ma J 2010 Cryst. Res. Technol. 45 219
[30] Murakami M, Sakai N, Higuchi T, Yoo S I 1996 Supercond. Sci. Technol. 9 1015
[31] Chen S Y, Hsiao Y S, Chen C L, Yan D C, Chen I G, Wu M K 2008 Mater. Sci. Eng. B 151 31
[32] Koblischka M R, Muralidhar M, Murakami M 1999 Mater. Sci. Eng. B 65 58
[33] Koblischka M R, van Dalen A J J, Higuchi T, Yoo S I, Murakami M 1998 Phys. Rev. B 58 2863
[34] Hinai H, Nariki S, Seo S J, Sakai N, Murakami M, Otsuka M 2000 Supercond. Sci. Technol. 13 676
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[1] Sha J J, Yao Z W, Yu J N, Yu G, Luo J H, Wen H H, Yang W L, Li S L 2000 Acta Phys. Sin. 49 1356 (in Chinese) [沙建军、姚仲文、郁金南、郁 刚、罗金汉、闻海虎、杨万里、李世亮 2000 物理学报 49 1356]
[2] Feng Y, Zhou L, Yang W M, Zhang C P, Wang J R, Yu Z M, Wu X Z 2000 Acta Phys. Sin. 49 146 (in Chinese) [冯 勇、周 廉、杨万民、张翠萍、汪京荣、于泽铭、吴晓祖 2000 物理学报 49 146]
[3] Cai Y Q, Yao X, Li G 2006 Acta Phys. Sin. 55 844 (in Chinese) [蔡衍卿、姚 忻、李 刚 2006 物理学报 55 844]
[4] Zhang Y L, Yao X, Zhang H, Jin Y P 2005 Acta Phys. Sin. 54 3380 (in Chinese) [张玉龙、姚 忻、张 宏、金燕苹 2005 物理学报 54 3380]
[5] Xu C Y, Shi L, Zuo J, Pang W H, Zhang Y L 1996 Acta Phys. Sin. 45 893 (in Chinese) [许存义、石 磊、左 健、庞文华、张裕恒 1996 物理学报 45 893]
[6] Zhou Z J, Zhou Z W, Zhou L Y, Lin L, Li X G, Feng Q R 2004 Chin. Phys. 13 1957
[7] Ding F Z, Lü X D, Gu H W, Li T, Cao J L 2009 Chin. Phys. B 18 1631
[8] Shen C X, Shen X L, Lu W, Dong X L, Li Z C, Xiong J W, Zhou F 2008 Chin. Phys. B 17 1425
[9] Shabna R, Sarun P M, Vinu S, Syamaprasad U 2009 Chin. Phys. B 18 4000
[10] Babu N H, Lo W, Cardwell D A, Campbell A M 1999 Appl. Phys. Lett. 75 2981
[11] Muralidhar M, Sakai N, Chikumoto N, Jirsa M, Machi T, Nishiyama M, Wu Y, Murakami M 2002 Phys. Rev. Lett. 89 237001
[12] Shen X L, Li Z C, Shen C X, Lu W, Dong X L, Zhou F, Zhao Z X 2009 Chin. Phys. B 18 2893
[13] Gawalek W, Habisreuther T, Zeisberger M, Litzkendorf D, Surzhenko O, Kracunovska S, Prikhna T A, Oswald B, Kovalev L K, Canders W 2004 Supercond. Sci. Technol. 17 1185
[14] Werfel F N, Floegel-Delor U, Rothfeld R, Goebel B, Wippich D, Riedel T 2005 Supercond. Sci. Technol. 18 S19
[15] Oswald B, Best K J, Setzer M, Soll M, Gawalek W, Gutt A, Kovalev L, Krabbes G, Fisher L, Freyhardt H C 2005 Supercond. Sci. Technol. 18 S24
[16] Dai J Q, Zhao Z X, Xiong J W 2003 Supercond. Sci. Technol. 16 815
[17] Babu N H, Iida K, Shi Y, Cardwell D A 2005 Appl. Phys. Lett. 87 202506
[18] Iida K, Babu N H, Shi Y, Cardwell D A 2005 Supercond. Sci. Technol. 18 1421
[19] Iida K, Babu N H, Shi Y, Cardwell D A 2006 Supercond. Sci. Technol. 19 S478
[20] Meslin S, Iida K, Babu N H, Cardwell D A, Noudem J G 2006 Supercond. Sci. Technol. 19 711
[21] Noudem J G, Meslin S, Horvath D, Harnois C, Chateigner D, Ouladdiaf B, Eve S, Gomina M, Chaud X, Murakami M 2007 J. Am. Ceram. Soc. 90 2784
[22] Li G Z, Yang W M 2010 Acta Phys. Sin. 59 5208 (in Chinese) [李国政、杨万民 2010 物理学报 59 5208]
[23] Varanasi C, Mcginn P J, Blackstead H A, Pullinga D B 1995 Appl. Phys. Lett. 67 1004
[24] Feng Y, Zhou L, Wen J G, Koshizuka N, Sulpice A, Tholence J L, Vallier J C, Monceau P 1998 Physica C 297 75
[25] Zheng H, Jiang M, Huang Y, Veal B W, Claus H 1998 Physica C 307 284
[26] Nariki S, Sakai N, Murakami M, Hirabayashi I 2004 Physica C 412-414 557
[27] Iida K, Babu N H, Withnell T D, Shi Y, Haindl S, Weber H W, Cardwell D A 2006 Physica C 445-448 277
[28] Babu N H, Iida K, Shi Y, Cardwell D A 2006 Physica C 445-448 286
[29] Li G Z, Yang W M, Tang Y L, Ma J 2010 Cryst. Res. Technol. 45 219
[30] Murakami M, Sakai N, Higuchi T, Yoo S I 1996 Supercond. Sci. Technol. 9 1015
[31] Chen S Y, Hsiao Y S, Chen C L, Yan D C, Chen I G, Wu M K 2008 Mater. Sci. Eng. B 151 31
[32] Koblischka M R, Muralidhar M, Murakami M 1999 Mater. Sci. Eng. B 65 58
[33] Koblischka M R, van Dalen A J J, Higuchi T, Yoo S I, Murakami M 1998 Phys. Rev. B 58 2863
[34] Hinai H, Nariki S, Seo S J, Sakai N, Murakami M, Otsuka M 2000 Supercond. Sci. Technol. 13 676
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