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Optical properties and laser damage performance of SiO2 irradiated by high-power pulsed electron beam

Zhong Mian Yang Liang Ren Wei Xiang Xia Liu Xiang Lian You-Yun Xu Shi-Zhen Guo De-Cheng Zheng Wan-Guo Yuan Xiao-Dong

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Optical properties and laser damage performance of SiO2 irradiated by high-power pulsed electron beam

Zhong Mian, Yang Liang, Ren Wei, Xiang Xia, Liu Xiang, Lian You-Yun, Xu Shi-Zhen, Guo De-Cheng, Zheng Wan-Guo, Yuan Xiao-Dong
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  • A 60 kW electron beam is used to study the microstructure and optical property evolutions as well as laser induced damage threshold of fused silica after irradiation at room temperature. Optical microscopic results indicate that cracks appear at the surface of SiO2 after electron beam irradiation, owing to the thermal effect, and that the crack density and size increase with increasing radiation dose. The morphology of the surface cracks is analyzed by using atomic force microscope and the width of crack is about 1 μm. In addition, there are a large number of debris particles with sizes of 0.1-1 μm on the surface. From the optical absorption spectrum of each of all samples, a weak absorption peak at 394 nm is observed and the absorbance increases at the beginning then decreases with increasing electron-radiation dose. Before and after irradiation, three absorption bands at 460 nm, 496 nm and 520 nm are clearly observed and their intensities first increase and then decrease, which is consistent with the results of absorption spectra. The effect of electron dose on the laser induced damage threshold (LIDT) at 355 nm is investigated and the results indicate that the LIDT decreases with increasing dose. At the lower electron doses, the color centers are responsible for the decrease of LIDT. However, at the higher electron doses, the decrease of LIDT is due to the light modulation and absorption induced by microscale cracks and debris particles at the surface of irradiated fused silica.
    • Funds: Project supported by the National Natural Science Foundation of China (Grant No. 61178018) and the Fundamental Research Fund for the Central Universities, China (Grant No. ZYGX2012J057).
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    [2]

    Ibarra A, Hodgson E R 2004 Nucl. Instrum. Meth. B 218 29

    [3]

    Yamamoto S, Shikama T, Belyakov V, Farnum E, Hodgson E, Nishitani T, Costley A, de Kock L, Walker C, Janeschitz G, 2000 J. Nucl. Mater. 283 60

    [4]

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    [5]

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    [6]

    Manzano J, Morono A, Hodgson E R 2009 Fusion Eng. Des. 84 1245

    [7]

    González S, Morono A, Hodgson E R 2005 Fusion Eng. Des. 74 831

    [8]

    León M, Martín P, Bravo D, López F, Ibarra A, Rascón A, Mota F 2008 J. Nucl. Mater. 374 386

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    León M, Martín P, Vila R, Molla J, Ibarra A 2009 Fusion Eng. Des. 84 1174

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    N uritdinov I, Masharipov K Y, Doniev M 2003 Glass Phys. Chem. 29 11

    [12]

    Cannas M, Agnello S, Gelardi F, Boscaino R, Trukhin A, Liblik P, Lushchik C, Kink M, Maksimov Y, Kink R 2004 J. Phys.: Condens. Matter 16 7931

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    Martín P, León M, Ibarra A, Hodgson E R 2011 J. Nucl. Mater. 417 818

    [14]

    Fitting H J, Barfels T, Von Czarnowski A, Trukhin A N 2000 Mater. Sci. Eng. B 71 109

    [15]

    D' Amico M, Messina F, Cannas M, Leone M, Boscaino R 2009 Phys. Rev. B 79 064203

    [16]

    Nuccio L, Agnello S, Boscaino R, Boizot B, Parlato A 2007 J. Non-Cryst. Solids 353 581

    [17]

    Zoubir A, Rivero C, Grodsky R, Richardson K, Richardson M, Cardinal T, Couzi M 2006 Phys. Rev. B 73 224117

    [18]

    Sergeev P B, Sergeev A P, Zvorykin V D 2007 Quantum Electron. 37 711

    [19]

    Sergeev P B, Sergeev A P 2010 Quantum Electron. 40 804

    [20]

    Guizard S, Martin P, Petite G, D'Oliveira P, Meynadier P 1996 J. Phys.: Condens. Matter 8 1281

    [21]

    Skuja L, Hirano M, Hosono H, Kajihara K 2005 Phys. Stat. Sol. 2 15

    [22]

    Griscom D L 1991 J. Ceram. Soc. Jpn. 99 923

    [23]

    Chen L, Wang T S, Zhang G F, Yang K J, Peng H B, Zhang L M 2013 Chin. Phys. B 22 126101

    [24]

    Lian Y Y, Liu X, Xu Z Y, Song J P, Yu Y 2013 Fusion Eng. Des. 88 1694

    [25]

    Chen X Q, Zu X T, Zheng W G, Jiang X D, L H B, Ren H, Zhang Y Z, Liu C M 2006 Acta Phys. Sin. 55 1201 (in Chinese) [陈习权, 祖小涛, 郑万国, 蒋晓东, 吕海兵, 任寰, 张艳珍, 刘春明 2006 物理学报 55 1201]

    [26]

    Wang P W, Kimberlin K R, Chengyu W, Ying T, Lin G Q, Aimin W, Jun X J 2005 Mater. Chem. Phys. 94 252

    [27]

    Skuja L 1994 J. Non-Cryst. Solids 167 229

    [28]

    Skuja L 1998 J. Non-Cryst. Solids 239 16

    [29]

    Skuja L, Streletsky A, Pakovich A 1984 Solid State Commun. 50 1069

    [30]

    Sakurai Y 2006 J. Non-Cryst. Solids 352 2917

    [31]

    Sakurai Y, Nagasawa K 2001 J. Non-Cryst. Solids 291 86

    [32]

    Wang F, Qin X F, Ren S H, Yang L X, Meng Y F, Ming Y F 2013 Mater. Res. Bull. 48 3640

    [33]

    Lin J, Huang Y, Zhang J, Gao J M, Ding X X, Huang Z X, Tang C C, Hu L, Chen D F 2007 Chem. Mater. 19 2585

    [34]

    Hua J R, Zu X T, Li L, Xiang X, Chen M, Jiang X D, Yuan X D, Zheng W G 2010 Acta Phys. Sin. 59 2519 (in Chinese) [花金荣, 祖小涛, 李莉, 向霞, 陈猛, 蒋晓东, 袁晓东, 郑万国 2010 物理学报 59 2519]

    [35]

    Hua J R, Li L, Xiang X, Zu X T 2011 Acta Phys. Sin. 60 044206 (in Chinese) [花金荣, 李莉, 向霞, 祖小涛 2011 物理学报 60 044206]

    [36]

    Jiang Y 2012 Ph. D. Dissertation (Chengdu: University of Electronic Science and Technology of China) (in Chinese) [蒋勇 2012 博士学位论文 (成都: 电子科技大学)]

  • [1]

    Holtkamp N 2007 Fusion Eng. Des. 82 427

    [2]

    Ibarra A, Hodgson E R 2004 Nucl. Instrum. Meth. B 218 29

    [3]

    Yamamoto S, Shikama T, Belyakov V, Farnum E, Hodgson E, Nishitani T, Costley A, de Kock L, Walker C, Janeschitz G, 2000 J. Nucl. Mater. 283 60

    [4]

    Campbell J H, Hawley-Fedder R A, Stolz C J, Menapace J A, Borden M R, Whitman P K, Yu J, Runkel M J, Riley M O, Feit M D 2004 Proc. SPIE 5341 San Jose, USA, January 24-29, 2004 p84

    [5]

    Devine R A 1993 J. Non-Cryst. Solids. 152 50

    [6]

    Manzano J, Morono A, Hodgson E R 2009 Fusion Eng. Des. 84 1245

    [7]

    González S, Morono A, Hodgson E R 2005 Fusion Eng. Des. 74 831

    [8]

    León M, Martín P, Bravo D, López F, Ibarra A, Rascón A, Mota F 2008 J. Nucl. Mater. 374 386

    [9]

    León M, Martín P, Vila R, Molla J, Ibarra A 2009 Fusion Eng. Des. 84 1174

    [10]

    Galeener F L, Kerwin D B, Miller A J, Mikkelsen J C 1993 Phys. Rev. B 47 7760

    [11]

    N uritdinov I, Masharipov K Y, Doniev M 2003 Glass Phys. Chem. 29 11

    [12]

    Cannas M, Agnello S, Gelardi F, Boscaino R, Trukhin A, Liblik P, Lushchik C, Kink M, Maksimov Y, Kink R 2004 J. Phys.: Condens. Matter 16 7931

    [13]

    Martín P, León M, Ibarra A, Hodgson E R 2011 J. Nucl. Mater. 417 818

    [14]

    Fitting H J, Barfels T, Von Czarnowski A, Trukhin A N 2000 Mater. Sci. Eng. B 71 109

    [15]

    D' Amico M, Messina F, Cannas M, Leone M, Boscaino R 2009 Phys. Rev. B 79 064203

    [16]

    Nuccio L, Agnello S, Boscaino R, Boizot B, Parlato A 2007 J. Non-Cryst. Solids 353 581

    [17]

    Zoubir A, Rivero C, Grodsky R, Richardson K, Richardson M, Cardinal T, Couzi M 2006 Phys. Rev. B 73 224117

    [18]

    Sergeev P B, Sergeev A P, Zvorykin V D 2007 Quantum Electron. 37 711

    [19]

    Sergeev P B, Sergeev A P 2010 Quantum Electron. 40 804

    [20]

    Guizard S, Martin P, Petite G, D'Oliveira P, Meynadier P 1996 J. Phys.: Condens. Matter 8 1281

    [21]

    Skuja L, Hirano M, Hosono H, Kajihara K 2005 Phys. Stat. Sol. 2 15

    [22]

    Griscom D L 1991 J. Ceram. Soc. Jpn. 99 923

    [23]

    Chen L, Wang T S, Zhang G F, Yang K J, Peng H B, Zhang L M 2013 Chin. Phys. B 22 126101

    [24]

    Lian Y Y, Liu X, Xu Z Y, Song J P, Yu Y 2013 Fusion Eng. Des. 88 1694

    [25]

    Chen X Q, Zu X T, Zheng W G, Jiang X D, L H B, Ren H, Zhang Y Z, Liu C M 2006 Acta Phys. Sin. 55 1201 (in Chinese) [陈习权, 祖小涛, 郑万国, 蒋晓东, 吕海兵, 任寰, 张艳珍, 刘春明 2006 物理学报 55 1201]

    [26]

    Wang P W, Kimberlin K R, Chengyu W, Ying T, Lin G Q, Aimin W, Jun X J 2005 Mater. Chem. Phys. 94 252

    [27]

    Skuja L 1994 J. Non-Cryst. Solids 167 229

    [28]

    Skuja L 1998 J. Non-Cryst. Solids 239 16

    [29]

    Skuja L, Streletsky A, Pakovich A 1984 Solid State Commun. 50 1069

    [30]

    Sakurai Y 2006 J. Non-Cryst. Solids 352 2917

    [31]

    Sakurai Y, Nagasawa K 2001 J. Non-Cryst. Solids 291 86

    [32]

    Wang F, Qin X F, Ren S H, Yang L X, Meng Y F, Ming Y F 2013 Mater. Res. Bull. 48 3640

    [33]

    Lin J, Huang Y, Zhang J, Gao J M, Ding X X, Huang Z X, Tang C C, Hu L, Chen D F 2007 Chem. Mater. 19 2585

    [34]

    Hua J R, Zu X T, Li L, Xiang X, Chen M, Jiang X D, Yuan X D, Zheng W G 2010 Acta Phys. Sin. 59 2519 (in Chinese) [花金荣, 祖小涛, 李莉, 向霞, 陈猛, 蒋晓东, 袁晓东, 郑万国 2010 物理学报 59 2519]

    [35]

    Hua J R, Li L, Xiang X, Zu X T 2011 Acta Phys. Sin. 60 044206 (in Chinese) [花金荣, 李莉, 向霞, 祖小涛 2011 物理学报 60 044206]

    [36]

    Jiang Y 2012 Ph. D. Dissertation (Chengdu: University of Electronic Science and Technology of China) (in Chinese) [蒋勇 2012 博士学位论文 (成都: 电子科技大学)]

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Publishing process
  • Received Date:  18 May 2014
  • Accepted Date:  08 July 2014
  • Published Online:  05 December 2014

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