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中国物理学会期刊

热压铁氧体的制备条件和磁性

CSTR: 32037.14.aps.23.1-3

PREPARATION AND MAGNETIC PROPERTIES OF HOT-PRESSED FERRITES

CSTR: 32037.14.aps.23.1-3
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  • 本文从实验上研究了起始粉料的制备方法和热压条件对磁头用的Mn-Zn及Ni-Zn热压铁氧体的密度、显微结构和磁性的影响。实验结果表明,化学共沉淀法制备的铁氧体粉料比氧化物法及硫酸盐法制备的要好。适当选择热压条件,可以获得晶粒分布均匀、晶粒大小不同(10μm—300μm)的高密度铁氧体;可以获得μ0=7420以及Bm=4950Gs的高密度Mn-Zn铁氧体和μ0等于100—2500的高密度Ni-Zn铁氧体。

     

    Experimental studies have been carried out on the effects of raw material preparation and hot-pressed conditions on the density, microstructure and magnetic properties of hot-pressed Mn-Zn ferrites and Ni-Zn ferrites which are used for magnetic head application. Hot-pressed ferrites have been prepared by two different technologies: the co-precipitation method and the ball-milling method. It was observed that the co-precipitation method is better than the ball-milling method for preparation of hot-pressed ferrites. The microstructure can be controlled by varying the hot-pressed conditions. Dense ferrites of different grain sizes (average grain size 10 μm-300 μm) can be made. For example, dense Mn-Zn ferrites with μ0 = 7420 and Bm = 4950 Gs and dense Ni-Zn ferrites with different μ0(μ0= 100-2500) can be made by hot-pressing.

     

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