搜索

x
中国物理学会期刊

直拉法生长的YAG单晶体中组分过冷引起的针状应力区和位错

CSTR: 32037.14.aps.30.218

THE NEEDLE-LIKE STRESS ZONES AND DISLOCATIONS DUE TO CONSTITUTIONAL SUPERCOOLING IN CZOCHRALSKI METHOD-GROWN YAG SINGLE CRYSTALS

CSTR: 32037.14.aps.30.218
PDF
导出引用
  • 本文研究了掺钕的YAG(Y3Al5O12)晶体在组分过冷条件下,固液界面的形态演变以及产生的钕离子的富集区。该富集区在正交偏光下表现为针状应力区。利用光弹方法确定了该应力为压应力,且应力分布具有圆柱对称性。通过浸蚀法和双折射貌相法观察到在钕富集区边界处存在位错列,并测定了位错的线密度。其结果与根据钕的浓度差值估计的密度大体符合。故认为这些位错是钕富集区边界处点阵失配所引起的。

     

    In this paper, we studied the relationship between the morphological development of the solid-liquid interface and the needle-like stress zones in Czochralskimethod-grown YAG single crystals doped with Nd. The experimental results established that the needle-like stress zones were originated from the solute (Nd) -rich zones due to constitutional supercooling. By studying the needle-like stress zones with photo-elasticity method, the stress in these zones was found to be axially symmetrical comperssive. We have also studied dislocation arrays along the boundaries of solute (Nd)-rich zones by means of etching method and birefringence observation, and measured the dis location density. The measured density agrees roughly with the value estimated according to the theory of misfit dislocations.

     

    目录

    /

    返回文章
    返回