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以附加记号法测定异垂盆草甙元的晶体结构时,出现了相位退化问题,由此得到同时混含两个对映体的E图,应用分量关系式成功地将这样的E图复原为只含一个对映体的E图。这一成功表明:使用附加记号法测定非中心对称的晶体结构,当出现相位退化时无需迴避,这就提高了附加记号法的使用效力。Phase degeneration occured during the solution of crystal structure of asosarmen-tosin by using symbolic addition procedure. This led to an E-map containing simultaneously both enantiomorphs. By making use of the component relation, this E-map has successfully been retrieved leading to an E-map containing only one of the enantiomorphs. It turns out that, with the help of component relation there is no need to modify the starting set even though phase degeneration occurs during the solution of noncentrosymmetric crystal structures by symbolic addition method. Hence the efficiency of the symbolic addition procedure can be improved.







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