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中国物理学会期刊

Bl结构MoNx薄膜的制备及物理性能研究

CSTR: 32037.14.aps.37.1089

THE PREPARATION AND PHYSICAL PROPERTIES OF B1 STRUCTURE MoNx THIN FILMS

CSTR: 32037.14.aps.37.1089
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  • 我们对以反应性溅射法制备的MoNx薄膜测量了超导转变温度Tc,电阻率ρ(T)(从Tc起始到300K)。用X射线衍射技术、卢瑟福背散射(RBS)、俄歇谱仪和X射线光电子能谱(XPS)技术对这些样品进行了分析。实验结果表明Tc和ρ(T)随N含量改变而变化。当样品是B1结构时,Tc小于4.2K,而且样品内还有过量的N存在。俄歇分析表明,样品内有O,C杂质存在。这些因素都可能导致Tc很低,ρ(T)呈负的温度系数。

     

    We have measured the superconducting transition temperature Tc and resistivity ρ(T) (from Tc onset to 300 K) of the reactive sputtered MoNx thin films. The X-ray diffraction, Rutherford back scattering (RBS), Auger and XPS technique were used for exmination of these specimens. The results showed that Tc and ρ(T) change with the concentration of nitrogen in thin films obviously. For Bl structure or nitrogen-rich samples, Tc is lower than 4.2 K. dρ/dT is negative as temperature is higher than Tc onset. Auger analysis indicated that the existence of oxygen and carbon could be also the reason for very low Tc and semiconducting behaviour in ρ(T) of this kind of thin films.

     

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