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中国物理学会期刊

利用场发射显微镜研究O2对单壁碳纳米管场发射的影响

CSTR: 32037.14.aps.52.1282

FEM study on the influence of oxygen on field emission of singlewalled carbon nanotubes

CSTR: 32037.14.aps.52.1282
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  • 利用场发射显微镜和四极质谱计研究了充入高纯O2的四极质谱和O2对单壁碳纳米管场发射的影响.单壁碳纳米管经过约1000℃的热处理得到清洁态场发射像后,充入O2,分别测量了O2吸附和脱附后场发射的IV特性.实验观测到在单壁碳纳米管上O2的吸附使场发射电流减小,说明逸出功增加.在10-4Pa的O2压强下对单壁碳纳米管进行约1000℃的热处理,可以产生氧化刻蚀作用,观测到场发射像的变化,并测量了氧化刻蚀产生的IV特性变化.

     

    Influence of oxygen on the field emission of singlewalled carbon nanotubes (SWCNTs) was studied using a fieldemission microscope (FEM) and a quadrupole mass spectrometer. After heat treatment at 1000℃, the field emission of clean SWCNTs occurred. Then oxygen was introduced into the vacuum system and the curves of field emission current versus anodecathode voltage (IV curves) were acquired after oxygen adsorption and desorption, respectively. We have observed that oxygen adsorption on SWCNTs leads to a decrease in field emission current, indicating an increase in the work function. Oxidation etching occurred when the SWCNTs were annealed at about 1000℃ under a pressure of 10-4Pa, and the corresponding changes were observed in both field emission images and IV curves.

     

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