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利用混合物理化学气相沉积法(HPCVD)在MgO(111)衬底上制备了干净的MgB2超导超薄膜. 在背景气体压强, 载气氢气流量以及沉积时间一定的情况下, 改变B2H6的流量, 制备得到不同厚度系列的MgB2超导薄膜样品, 并测量了其超导转变温度 Tc, 临界电流密度Jc等临界参量. 该系列超导薄膜沿c轴外延生长, 表面具有良好的连接性, 且有很高的超导转变温度Tc(0) ≈ 35-38 K和很小的剩余电阻率ρ(42 K) ≈ 1.8-20.3 μΩ·cm-1. 随着膜厚的减小而减小, 临界温度变低, 而剩余电阻率变大. 其中20 nm的样品在零磁场, 5K时的临界电流密度Jc ≈ 2.3×107 A/cm2. 表明了利用HPCVD在MgO(111)衬底上制备的MgB2超薄膜有很好的性能, 预示了其在超导电子器件中广阔的应用前景.
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关键词:
- MgO(111)衬底 /
- MgB2超薄膜 /
- 混合物理化学气相沉积
We fabricate MgB2 ultra-thin films via hybrid physics-chemical vapor deposition technique (HPCVD). Under the same background pressure, the same H2 flow rate and the same deposition time, by changing the B2H6 flow rate, we fabricate a series of ultra-thin films with thickness values ranging from 10 nm to 40 nm. These films grow on MgO(111) substrate, and are all c-axis epitaxial. These films show the good connectivity, a very high Tc(0) ≈ 35-38 K and a very low residual resistivity ρ(42 K) ≈ 1.8-20.3 μΩ·cm-1. As the thickness increases, critical transition temperature also increases and the residual resistivity decreases. The 20 nm film also shows an extremely high critical current density Jc (0 T, 5 K) ≈ 2.3×107 A/cm2, which indicates that the films fabricated by HPCVD are well qualified for device applications.







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