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NiTi合金中应力诱导的I/C相变及其界面动力学的研究

张进修 李江宏

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NiTi合金中应力诱导的I/C相变及其界面动力学的研究

张进修, 李江宏

THE STUDIES OF STRESS-INDUCED I/C TRANSITION AND INTERFACE DYNAMICS IN NiTi ALLOY

ZHANG JIN-XIU, LI JIANG-HONG
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  • 在改装了的拉力试验机上,以不同的拉伸速率ε(0.79—18×10-5s-1)进行加、卸载试验,并用中间扭摆和四端电位法同时测量了Ni-49at%Ti合金丝在应力诱导I/C相变过程的内耗Q-1、模量M/M0、电阻率ρ/ρ0和应力-应变曲线。研究了应力循环和应变速率的影响。在Q-1-ε曲线上出现Q-1峰,而在f2-ε曲线上出现与之相对应的模量极小。内耗峰的高度Qp-1和模量亏损值均随ε增大而增大。根据界面动力学模型和内耗的实验数据,计算得应力诱导I/C相变过程界面的动力学关系为V=V*(△G—△GR)m,V*和m为动力学参数,△GR为相变过程中运动相界面所受的阻力,计算得△GR≈1cal/mol。讨论了内耗和模量亏损、软模效应之间的关系。
    The internal friction (IF) Q-1, modulus f2, electrical resistance R and stress s of superelastic Ni51Ti49 alloy in the process of stress induced incommensurate/commensurate (I/C) transition was measured as a function of strain e by a middle torsion pendulum on a tensile testing machihe modified with a four-terminal potential equipment.The effects of number of stress cycles and strain rate e (in the range of 7×10-7/s to 1×10-4/s) were studied. An IF peak and a minimum of modulus were observed respectively in the Q-1-εand f2-εcurves. The IF peak height Qp-1 and modulus defect △M/M increase with an increasing of ε/ω, where ω is angular frequency of measuring. By utilizing an expression obtained from phase interface dynamics and experimental data of Qp-1 (as a function of ε/ω and amount of phase transition F), an explicit functional relationship of average I/C phase interface velocity V and effective phase transition driving force △G′= △G - △GR (where △GR is resistance) was derived as V =V*(△G - △CR)m, where V* and m are dynamic parameters an △GR is a resistance force exerting on the moving interface, which has the order of 1 cal/mol for stress-induced I/C transition of superelastisity NiTi alloy. The relationship between Q-1 and modulus defect △M/M and soft modulus effect are disussed.
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  • 文章访问数:  6077
  • PDF下载量:  606
  • 被引次数: 0
出版历程
  • 收稿日期:  1985-12-31
  • 修回日期:  1987-03-12
  • 刊出日期:  2005-07-05

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