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中国物理学会期刊

基于CT成像技术研究振动状态下的颗粒堆积的老化

Aging of Tapped Granular Packing Using CT Imaging

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  • 颗粒物质广泛存在于自然界与工业过程中,其独特的物理性质和行为一直是物理学研究的热点。颗粒堆积作为颗粒物理中的重要课题,对工业生产具有显著的实际意义。其中,球形颗粒因具有高度对称性和简单的几何特征,成为研究颗粒堆积问题最为理想的模型。本研究通过激振器对颗粒体系施加持续的外部振动激励,结合X射线断层扫描技术、分水岭图像处理算法以及Voronoi划分方法,获取了不同时刻体系的堆积密度。结果表明,在不同振动强度下,颗粒堆积密度随振动次数的变化均符合Kohlrausch-Williams-Watts(KWW)函数的拟合规律。同时发现,稳态堆积密度与振动强度之间存在非单调关系,说明外部激励并非单纯“加速致密化”,而可能改变了体系的可达构型空间和颗粒重排路径。为揭示上述非单调性背后的结构机制,本文引入了接触数与Minkowski张量等结构表征量进行分析。研究发现,即使在不同振动强度下体系达到相同的堆积密度,其内部结构在尺度与形态特征上仍表现出明显差异。进一步通过计算相关热力学量并结合Adam-Gibbs(AG)关系,发现在堆积密度转折点处AG关系同样发生转折。推测该现象可能与弛豫方式的转变有关:在较高振动强度下,颗粒弛豫主要由惯性振动主导;随着振动强度降低,弛豫方式逐渐转变为振动驱动的惯性运动与接触滑移共存的阶段;最终在振动强度极低时,弛豫完全由颗粒间的接触滑移主导。以上结果不仅为理解颗粒物质的老化行为提供了重要实验依据,也表明在不同振动条件下颗粒体系可能存在多种弛豫机制,对相关领域的进一步研究具有启示意义。

     

    Granular matter is ubiquitous in both natural and industrial settings, and its unique physical properties have long been a focus of research. As a central theme in this field, granular packing is of particular significance due to its direct relevance to industrial applications. Among various particle shapes, spheres, owing to their high symmetry and geometric simplicity, serve as the most ideal model for investigating packing problems.
    In this study, the granular packing was subjected to continuous external vibration by tapping. The volume fraction at different times was obtained by combining X-ray tomography with Watershed image processing algorithms and Voronoi tessellation.
    The results show that under different vibration intensities, the relationship between volume fraction and the number of vibrations is described by the Kohlrausch–Williams–Watts (KWW) function. However, a non-monotonic relationship was observed between the steady-state volume fraction and vibration intensity, indicating that external excitation does not simply "accelerate densification" but may also alter the accessible configuration space and rearrangement pathways of the system. To uncover the structural mechanisms behind this non-monotonic behavior, we introduced structural descriptors such as contact number and Minkowski tensors. The analysis revealed that even when systems reach the same volume fraction under different vibration intensities, their internal structures exhibit significant differences in their scale and morphological features. By further calculating relevant thermodynamic quantities and combining with the Adam–Gibbs (AG) relation, we find that a crossover in the AG relation occurs at the turning point of the volume fraction. This phenomenon is hypothesized to be related to a transition in relaxation mechanisms: at higher vibration intensities, granular packing relaxation is dominated by inertial vibration; as vibration intensity decreases, relaxation shifts to a combination of vibration-driven inertial motion and contact sliding; and at very low vibration intensities, relaxation becomes entirely governed by interparticle contact sliding. These findings not only provide important experimental evidence for understanding the aging behavior of granular materials but also suggest that multiple relaxation mechanisms may exist in granular systems under different vibrational conditions, offering insights for further research in related fields.

     

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