基于激光诱导击穿光谱技术的铝合金成分定量分析

孙对兄; 苏茂根; 董晨钟; 王向丽; 张大成; 马新文

doi:10.7498/aps.59.4571

摘要

利用Nd: YAG激光器输出的532 nm激光束对位于空气中的标准变形铝合金样品进行烧蚀产生了激光诱导等离子体.对测量的230—440 nm波长范围的光谱进行了谱线标定,同时基于自由定标方法对样品成分进行了定量分析,确定了样品中的元素含量.分析结果与标准值具有较好的一致性.

关键词:

Laser-induced breakdown plasma is produced by using Q-switched Nd: YAG laser operating at 532 nm, which interacts with the Al alloy sample target in air. The spectral lines in the 230—440 nm wavelength range have been identified, and based on the calibration-free method, the mass concentration of Al alloy are obtained, which is in good agreement with the standard value of the sample.

Keywords:

作者及机构信息

(1)西北师范大学物理与电子工程学院,兰州 730070; (2)中国科学院近代物理研究所,兰州 730000

基金项目: 国家自然科学基金(批准号:10774122,10876028)、高等学校博士学科点专项科研基金(批准号:20070736001)、兰州重离子加速器国家实验室原子核理论中心基金和西北师范大学科技创新工程基金(批准号:NWNU-KJCXGC-03-21)资助的课题.

Authors and contacts

(1)College of Physics and Electronic Engineering, Northwest Normal University, Lanzhou 730070, China; (2)Institute of Modern Physics, Chinese Academy of Sciences, Lanzhou 730000, China

参考文献

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[3]	St-Onge L, Kwong E, Sabsabi M, Vadas E B 2002 Spectrochim. Acta B 57 1131
[4]	Charfi B, Harith M A 2002 Spectrochim. Acta B 57 1141
[5]	de Giacomo A, Dell’Aglio M, Colao F, Fantoni R 2004 Spectrochim. Acta B 59 1431
[6]	de Giacomo A, Dell’ Aglio M, Depascale O 2004 Appl.Phys. A-Mater. 79 1035
[7]	Ciucci A, Palleschi V, Rastelli S, Barbini R, Colao F, Fantoni R, Palucci A, Ribezzo S 1996 Appl. Phys. B-Lasers O. 63 185
[8]	Cremers D A, Radziemski L J 2006 Handbook of Laser-Induced Breakdown Spectroscopy (Chichester: John Wiley & Sons) p137
[9]	Miles B, Cortes J 1998 Field Anal. Chem.Technol. 2 75
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[11]	Yuan D Q, Zhou M, Liu C L, Yan F, Dai J, Ren N F 2008 Spectrosc. Spect. Anal. 28 2019 (in Chinese) [袁冬青、周明、刘长隆、言峰、戴娟、任乃飞 2008 光谱学与光谱分析 28 2019]
[12]	Jin Z, Zhang J 2001 Acta Phys. Sin. 50 1022 (in Chinese)[金展、张杰 2001 物理学报 50 1022] 〖13] Lin Z X, Chang L, Li J, Liu L M 2009 Spectrosc. Spect. Anal. 29 1675 (in Chinese) [林兆祥、常亮、李捷、刘林美 2009 光谱学与光谱分析 29 1675]
[13]	Chen Z J, Li H K, Liu M, Li R H 2008 Spectrochim. Acta B 63 64
[14]	Cui Z F, Zhang X Y, Yao G X, Wang X L, Xu X S, Zheng X F, Feng E Y, Ji X H 2006 Acta Phys.Sin. 55 4506 (in Chinese) [崔执凤、张先燚、姚关心、汪小丽、许新胜、郑贤锋、凤尔银、季学韩 2006 物理学报 55 4506]
[15]	Bulajic D, Corsi M, Cristoforettii G, Legnaioli S, Palleschi V, Salvetti A, Tognoni E 2002 Spectrochim. Acta B 57 339
[16]	Lazic V, Barbini R, Colao F, Fantoni R, Palucci A 2001 Spectrochim. Acta B 56 807
[17]	Gornushkin I B, Anzano J M, King L A, Smith B W, Omenetto N, Winefordner J D 1999 Spectrochim. Acta B 54 491
[18]	Pavel Y, Doug B, Morrison R, Chadwick B 2006 Spectrochim. Acta B 61 200
[19]	Cristian A D, Diego M D, Graciela B, Daniela B 2008 Spectrochim. Acta B 63 367
[20]	Huddlestone R H, Leonard S L 1965 Plasma Diagnostics Techniques (New York: Academic Press) p48
[21]	Ciucci A, Palleschi V, Rastelli S, Tognoni E 1999 Appl. Spectrosc. 53 960
[22]	Fantoni R, Caneve L, Colao F, Fornarini L, Lazic V, Spizzichino V 2008 Spectrochim. Acta B 63 1097

施引文献

[1]	Adrain R S, Watson J 1984 J. Phys. D: Appl. Phys. 17 1915
[2]	Zaspu Y R, Kireev S V, Protsenko E D, Veselow V K 1992 Appl. Spectrosc. 56 116
[3]	St-Onge L, Kwong E, Sabsabi M, Vadas E B 2002 Spectrochim. Acta B 57 1131
[4]	Charfi B, Harith M A 2002 Spectrochim. Acta B 57 1141
[5]	de Giacomo A, Dell’Aglio M, Colao F, Fantoni R 2004 Spectrochim. Acta B 59 1431
[6]	de Giacomo A, Dell’ Aglio M, Depascale O 2004 Appl.Phys. A-Mater. 79 1035
[7]	Ciucci A, Palleschi V, Rastelli S, Barbini R, Colao F, Fantoni R, Palucci A, Ribezzo S 1996 Appl. Phys. B-Lasers O. 63 185
[8]	Cremers D A, Radziemski L J 2006 Handbook of Laser-Induced Breakdown Spectroscopy (Chichester: John Wiley & Sons) p137
[9]	Miles B, Cortes J 1998 Field Anal. Chem.Technol. 2 75
[10]	Bian B M, Chen J P, Yang L 2000 Acta Phys. Sin. 49 445 (in Chinese) [卞保民、陈建平、杨玲 2000 物理学报 49 445]
[11]	Yuan D Q, Zhou M, Liu C L, Yan F, Dai J, Ren N F 2008 Spectrosc. Spect. Anal. 28 2019 (in Chinese) [袁冬青、周明、刘长隆、言峰、戴娟、任乃飞 2008 光谱学与光谱分析 28 2019]
[12]	Jin Z, Zhang J 2001 Acta Phys. Sin. 50 1022 (in Chinese)[金展、张杰 2001 物理学报 50 1022] 〖13] Lin Z X, Chang L, Li J, Liu L M 2009 Spectrosc. Spect. Anal. 29 1675 (in Chinese) [林兆祥、常亮、李捷、刘林美 2009 光谱学与光谱分析 29 1675]
[13]	Chen Z J, Li H K, Liu M, Li R H 2008 Spectrochim. Acta B 63 64
[14]	Cui Z F, Zhang X Y, Yao G X, Wang X L, Xu X S, Zheng X F, Feng E Y, Ji X H 2006 Acta Phys.Sin. 55 4506 (in Chinese) [崔执凤、张先燚、姚关心、汪小丽、许新胜、郑贤锋、凤尔银、季学韩 2006 物理学报 55 4506]
[15]	Bulajic D, Corsi M, Cristoforettii G, Legnaioli S, Palleschi V, Salvetti A, Tognoni E 2002 Spectrochim. Acta B 57 339
[16]	Lazic V, Barbini R, Colao F, Fantoni R, Palucci A 2001 Spectrochim. Acta B 56 807
[17]	Gornushkin I B, Anzano J M, King L A, Smith B W, Omenetto N, Winefordner J D 1999 Spectrochim. Acta B 54 491
[18]	Pavel Y, Doug B, Morrison R, Chadwick B 2006 Spectrochim. Acta B 61 200
[19]	Cristian A D, Diego M D, Graciela B, Daniela B 2008 Spectrochim. Acta B 63 367
[20]	Huddlestone R H, Leonard S L 1965 Plasma Diagnostics Techniques (New York: Academic Press) p48
[21]	Ciucci A, Palleschi V, Rastelli S, Tognoni E 1999 Appl. Spectrosc. 53 960
[22]	Fantoni R, Caneve L, Colao F, Fornarini L, Lazic V, Spizzichino V 2008 Spectrochim. Acta B 63 1097

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