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中国物理学会期刊

邻苯二甲酸二甲酯晶体中裂纹愈合效应的力学谱研究

CSTR: 32037.14.aps.59.2120

Study of crack healing effect in dimethyl phthalate crystals by mechanical spectroscopy

CSTR: 32037.14.aps.59.2120
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  • 推广应用应力诱导裂纹和裂纹愈合的新方法(RMS-CH方法,Wu等,Appl. Phys. Lett. 92 011918-1(2008))于晶体材料的应力诱导裂纹和裂纹愈合过程的实时检测.对邻苯二甲酸二甲酯晶体的测量结果表明,在定升温速率条件下:1)裂纹愈合的速率随温度变化表现为较为尖锐的单峰,对应的峰温可以作为裂纹愈合的特征温度Tcch,且Tcch=206 K;2)裂纹愈合速率峰是不对称的

     

    The recently developed method to detect the stress-cracking and crack healing of glasses in real-time (called the RMS-CH in short,Wu et al.,Appl. Phys. Lett. 92,011918-1(2008)) is applied to the detections of crystals. The experimental results of dimethyl phthalate crystal indicate that,under the condition of constant heating rate:1) the crack-healing rate shows a sharp peak as a function of temperature,the peak temperature can be taken as the characteristic temperature Tcch of the crack-healing ,and Tcch=206 K;2) the peak is not symmetric,and the low temperature side is wider than the high temperature side,which means that the crack-healing has started at lower temperatures and the amount of healing below Tcch is more than that above Tcch. This behavior is similar to that in glasses,but Tcch is higher than that of glassy state. Moreover,Tcch is much lower than the melting point of the crystal,which indicates that the crack-healing mechanism is quite different from that of recrystallization. We would like to point out that two dynamical loss peaks related to the crack-healing process are observed for the first time,which will be helpful to the understanding of the mechanisms. The above results also show the feasibility and validity of the RMS-CH method to investigate the stress-cracking and crack-healing in crystals as in glasses.

     

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