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Evolution of surface relief and its intrinsic mechanism associated with martensitic transformation (MT) during heating and cooling in Mn79.5Fe15.6Cu4.9 high-temperature antiferromagnetic shape memory alloy (SMA) have been investigated in nano-scale by means of in-situ atomic force microscopy (AFM), X-ray diffraction (XRD), and dynamic mechanical analyzer (DMA). Experimental results show that the N-type surface relief originates from the reverse MT and is completely made of matrix which is different from the conventional ones. The reverse MT exhibits untwinning shear and the reverse shearing of twinned martensites mainly contribute to the surface relief. The measured surface relief angles are less than 1°, which are determined by the small difference of lattice constants between fcc and fct structures. Surface relief has a good recovery property because of the crystallographic reversibility rule in SMAs, implying that this kind of alloy has a good surface morphology memory effect.
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Keywords:
- surface relief /
- in-situ AFM /
- reverse martensitic transformation /
- Mn-Fe-Cu antiferromagnetic alloy
[1] Gong C W, Wang Y N, Yang D Z 2006 Acta Phys. Sin. 55 2877 (in Chinese) [宫长伟, 王佚农, 杨大智 2006 物理学报 55 2877]
[2] Manosa L, Gonzalez-Alonso D, Planes A, Bonnot E, Barrio M, Tamarit JL, Aksoy S, Acet M 2010 Nat. Mater. 9 478
[3] Peng W Y, Tan J, Zhang A S, Yan M M 2010 Acta Phys. Sin. 59 8244 (in Chinese) [彭文屹, 覃金, 章爱生, 严明明 2010 物理学报 59 8244]
[4] Zhang Y Z, Cao J M, Tan C L, Cao Y J, Cai W 2014 Chin. Phys. B 23 037504
[5] Wang D H, Han Z D, Xuan H C, Ma S C, Chen S Y, Zhang C L, Du YW 2013 Chin. Phys. B 22 077506
[6] Zhou Y, Wang H B, Wang G P 2011 Acta Phys. Sin. 60 107501 (in Chinese) [周英, 王海波, 王古平 2011 物理学报 60 107501]
[7] Efstathiou C, Sehitoglu H, Carroll J, Lambros J, Maier HJ 2008 Acta Mater. 56 3791
[8] Omori T, Sutou Y, Oikawa K, Kainuma R, Ishida K 2005 Scripta Mater. 52 565
[9] Zhang J H 2005 Curr Opin Solid State & Mater Sci. 9 326
[10] Zhang J H, Peng W Y, Hsu TY 2008 Appl. Phys. Lett. 93 122510
[11] Peng W Y 2007 Ph. D Dissertation (Shanghai: Shanghai Jiao Tong University) (in Chinese) [彭文屹 2007 博士学位论文(上海: 上海交通大学)]
[12] Tsunoda Y, Wakabayashi N 1981 J. Phys. Soc. Jpn. 50 3341
[13] Oguchi T, Freeman AJ 1984 J. Magn. Magn. Mater. 1-2 L1
[14] Xu Zuyao 1999 Martensitic Transformation and Martensite (2rd Ed.) (Beijing: Science Press) p9 (in Chinese) [徐祖耀 1999 马氏体相变与马氏体(第2版) (北京:科学出版社)第9页]
[15] Fang H S 1999 Bainitic Transformaiton (Beijing: Science Press) p254 (in Chinese) [方鸿生 1999 贝氏体相变(北京: 科学出版社) 第254页]
[16] Zhang J H, Rong Y H, Hsu TY 2010 varPhil Magazine. 90 159
[17] Ito K, Tsukishima M, Kobayashi M 1983 JIM 24 487
[18] Wang L T, Ge T S 1988 Acta Metall Sin. A 24 147 (in Chinese) [王力田, 葛庭燧 1988 金属学报 24 147]
[19] Waitz T, Karnthaler H P 1997 Acta Mater. 45 837
[20] Bergeon N, Kajiwara S, Kikuchi T 2000 Acta Mater. 48 4053
[21] Reinhold M, Waston C, Knowlton WB, M€ullner P 2010 J Appl Phys. 107 113501
[22] Liu D Z, Dunne D 2003 Scr Mater. 48 1611
[23] Yang Z G, Fang H S, Wang J J, Li C M, Zheng Y K 1995 Phys Rev. B 52 7879
[24] Tian Q C, Yin F X, Sakaguchi T, Nagai K 2006 Acta Mater. 54 1805
[25] Shimizu K, Okumura K, Kubo H 1982 Trans. JIM 23 53
[26] Wang Y, Zhang J H 2007 Acta Mater. 55 5169
[27] Artemev A, Wang Y, Khachaturyan AQ 2000 Acta Mater. 48 2503
[28] Liu D Z, Kajiwara S, Kikuchi T, Shinya N 2003 Philos Mag. 83 2875
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[1] Gong C W, Wang Y N, Yang D Z 2006 Acta Phys. Sin. 55 2877 (in Chinese) [宫长伟, 王佚农, 杨大智 2006 物理学报 55 2877]
[2] Manosa L, Gonzalez-Alonso D, Planes A, Bonnot E, Barrio M, Tamarit JL, Aksoy S, Acet M 2010 Nat. Mater. 9 478
[3] Peng W Y, Tan J, Zhang A S, Yan M M 2010 Acta Phys. Sin. 59 8244 (in Chinese) [彭文屹, 覃金, 章爱生, 严明明 2010 物理学报 59 8244]
[4] Zhang Y Z, Cao J M, Tan C L, Cao Y J, Cai W 2014 Chin. Phys. B 23 037504
[5] Wang D H, Han Z D, Xuan H C, Ma S C, Chen S Y, Zhang C L, Du YW 2013 Chin. Phys. B 22 077506
[6] Zhou Y, Wang H B, Wang G P 2011 Acta Phys. Sin. 60 107501 (in Chinese) [周英, 王海波, 王古平 2011 物理学报 60 107501]
[7] Efstathiou C, Sehitoglu H, Carroll J, Lambros J, Maier HJ 2008 Acta Mater. 56 3791
[8] Omori T, Sutou Y, Oikawa K, Kainuma R, Ishida K 2005 Scripta Mater. 52 565
[9] Zhang J H 2005 Curr Opin Solid State & Mater Sci. 9 326
[10] Zhang J H, Peng W Y, Hsu TY 2008 Appl. Phys. Lett. 93 122510
[11] Peng W Y 2007 Ph. D Dissertation (Shanghai: Shanghai Jiao Tong University) (in Chinese) [彭文屹 2007 博士学位论文(上海: 上海交通大学)]
[12] Tsunoda Y, Wakabayashi N 1981 J. Phys. Soc. Jpn. 50 3341
[13] Oguchi T, Freeman AJ 1984 J. Magn. Magn. Mater. 1-2 L1
[14] Xu Zuyao 1999 Martensitic Transformation and Martensite (2rd Ed.) (Beijing: Science Press) p9 (in Chinese) [徐祖耀 1999 马氏体相变与马氏体(第2版) (北京:科学出版社)第9页]
[15] Fang H S 1999 Bainitic Transformaiton (Beijing: Science Press) p254 (in Chinese) [方鸿生 1999 贝氏体相变(北京: 科学出版社) 第254页]
[16] Zhang J H, Rong Y H, Hsu TY 2010 varPhil Magazine. 90 159
[17] Ito K, Tsukishima M, Kobayashi M 1983 JIM 24 487
[18] Wang L T, Ge T S 1988 Acta Metall Sin. A 24 147 (in Chinese) [王力田, 葛庭燧 1988 金属学报 24 147]
[19] Waitz T, Karnthaler H P 1997 Acta Mater. 45 837
[20] Bergeon N, Kajiwara S, Kikuchi T 2000 Acta Mater. 48 4053
[21] Reinhold M, Waston C, Knowlton WB, M€ullner P 2010 J Appl Phys. 107 113501
[22] Liu D Z, Dunne D 2003 Scr Mater. 48 1611
[23] Yang Z G, Fang H S, Wang J J, Li C M, Zheng Y K 1995 Phys Rev. B 52 7879
[24] Tian Q C, Yin F X, Sakaguchi T, Nagai K 2006 Acta Mater. 54 1805
[25] Shimizu K, Okumura K, Kubo H 1982 Trans. JIM 23 53
[26] Wang Y, Zhang J H 2007 Acta Mater. 55 5169
[27] Artemev A, Wang Y, Khachaturyan AQ 2000 Acta Mater. 48 2503
[28] Liu D Z, Kajiwara S, Kikuchi T, Shinya N 2003 Philos Mag. 83 2875
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