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Yb:CaF2-SrF2激光晶体光谱性能以及热学性能的研究

吴叶青 苏良碧 徐军 陈红兵 李红军 郑丽和 王庆国

Yb:CaF2-SrF2激光晶体光谱性能以及热学性能的研究

吴叶青, 苏良碧, 徐军, 陈红兵, 李红军, 郑丽和, 王庆国
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  • 采用坩埚下降法生长了Yb: CaF2-SrF2晶体,测试了该晶体的吸收和荧光光谱 以及在不同温度下晶体的热扩散系数和热膨胀系数,并且计算了晶体的热膨胀系数以及在常温下的热导率. 采用对比的方法,对晶体的吸收光谱,荧光光谱,热学性能进行了分析.从吸收和荧光光谱结果表明: 在掺杂相对较高浓度的SrF2的混晶中, Yb3+吸收截面和发射截面比较大. Yb: CaF2-SrF2 (19%)晶体在1040 nm附近的发射截面比较大,光谱也比较宽. 这说明在掺杂相同浓度Yb时,混晶中CaF2, SrF2的比例不同,晶体的光谱性质不同, 主要原因是在混晶中晶体的无序度不同,晶体对称性降低,形成低对称光学中心. 从热扩散系数计算的热导率结果看出晶体具有比较好的热导率.
    • 基金项目: 国家自然科学基金(批准号: 60938001, 60908030, 61178056)资助的课题.
    [1]

    Haumesser P H, Gaumé R, Benitez J M, Viana B, Ferrand B, Aka G, Vivien D 2001 J. Cryst. Growth 233 233

    [2]

    Chénais S, Druon F, Balembois F, Georges P, Gaumé R, Haumesser P H, Viana B, Aka G P, Vivien D 2002 J. Opt. Sco. Am. B 19 1083

    [3]

    Haumesser P H, Gaumé R, Viana B, Vivien D 2002 J. Opt. Soc. Am. B 19 2365

    [4]

    Jiang H D, Wang J Y, Zhang H J, Hu X B, Burns P, A Piper J, Piper J A 2002 Chem. Phys. Lett. 361 493

    [5]

    Lebedev V A, Voroshilov I V, Ignatiev B V, Gavrilenko A N, Isaev V A, Shestakov A V 2001 J. Lumin 92 139

    [6]

    Li P X, Zou S Z, Zhang X X, Li G 2010 Chin. Phys. B 19 074211

    [7]

    Wang S M, Du S F, Lu J, Zhang D X, Feng B H 2007 Chin. Phys. Soc. 1786-04

    [8]

    Kong L J, Xiao X S, Yang C X 2010 Chin. Phys. B 19 074212

    [9]

    Siebold M, Bock S, Schramm U, Xu B, Doualan J L, Camy P, Moncorgé R 2009 Appl. Phys. B 97 327

    [10]

    Ricaud S, Papadopoulos D N, Pellegrina A, Balembois F, Georges P, Courjaud A, Camy P, Doualan J L, Moncorgé R, Druon F 2011 Opt. Lett. 36 1602

    [11]

    Lucca A, Debourg G, Jacquemet M, Druon F, Balembois F, Georges P, Camy P, Doualan J L, Moncorgé R 2004 Opt. Lett. 29 2767

    [12]

    Ricaud S, Papadopoulos D N, Camy P, Doualan J L, Moncorgé R, Courjaud A, Mottay E, Georges P, Druon F 2010 Opt. Lett. 35 3757

    [13]

    Ricaud S, Druon F, Papadopoulos D N, Camy P, Doualan J L, Moncorgé R, Delaigue M, Zaouter Y, Courjaud A, Georges P, Mottay E 2010 Opt. Lett. 35 2415

    [14]

    Siebold M, Hein J, Kaluza M C, Uecker R 2007 Opt. Lett. 32 1818

    [15]

    Silva M A P, Messaddeq Y, Briois V, Poulain M, Villain F, Ribeiro S J L 2002 Solid State Ionics 147 135

    [16]

    Sorokin N I, Buchinskaya I I, Fedorov P P, Sobolev B P 2008 Inorg. Mater. 44 234

    [17]

    Karimov D N, Komar'kova O N, Sorokin N I, Bezhanov V A, Chernov S P, Popov P A, Sobolev B P 2010 Crystallogr. Rep. 55 518

    [18]

    Mouchovski J T, Temelkov K A, Vuchkov N K 2011 Prog. Cryst. Growth Charact Mater 57 1

    [19]

    Klimma D, Rabe M, Bertrama R, Uecker R, Parthier L 2008 J. Cryst. Growth 310 152

    [20]

    Basiev T T, Vasil'ev S V, Doroshenko M E, Konyushkin V A, Kuznetsov S V, Osiko V V, Fedorov P P 2007 Quant. Electron 37 934

    [21]

    Basiev T T, Doroshenko M, Fedorov P, Konyushkin V A, Kuznetsov S, Osiko V, Akchurin M 2008 Opt. Lett. 33 521

    [22]

    Basiev T T, Doroshenko M, Konyushkin V A 2011 Advances in Optical Materials (AIOM) paper: AIThA3

    [23]

    Youngmen R E, Smith C M 2008 Phys. Rev. B 78 014112

    [24]

    Fedorov P P, Osiko V V, Basiev T T, Orlovskii Yu V, Dukel'skii K V, Mironov I A, Demidenko V A, Smirnov A N 2007 Nanotechnologies in Russia 2 95

    [25]

    Siebold M, Bock S, Schramm U, Xu B, Doualan J L, Camy P, Moncorgé R 2009 Appl. Phys. B 97 327

    [26]

    Alimov O K, Basiev T T, Doroshenko M E, Fedorov P P, Konyushkin V A, Kouznetsov S V, Nakladov A N, Osiko V V, Jelinkova H, Šulc J 2009 Advanced Solid-State Photonics, OSA Technical Digest Series (CD) (Optical Society of America). paper WB25

    [27]

    Zeng X H, Zhao G J, Xu X D, Li H J, Xu J, Zhao Z W, He X M, Pang H Y, Jie M Y, Yan C F 2005 J. Cryst. Growth 274 106

    [28]

    Yu Y G, Wang J Y, Zhang H J, Wang Z P, Yu H H, Sun S Q, Xia H R, Jiang M H 2009 Opt. Express 17 9270

    [29]

    Ge W, Zhang H, Wang J, Liu J, Xu X, Hu X, Jiang M 2005 J. Appl. Phys. 98 013542

  • [1]

    Haumesser P H, Gaumé R, Benitez J M, Viana B, Ferrand B, Aka G, Vivien D 2001 J. Cryst. Growth 233 233

    [2]

    Chénais S, Druon F, Balembois F, Georges P, Gaumé R, Haumesser P H, Viana B, Aka G P, Vivien D 2002 J. Opt. Sco. Am. B 19 1083

    [3]

    Haumesser P H, Gaumé R, Viana B, Vivien D 2002 J. Opt. Soc. Am. B 19 2365

    [4]

    Jiang H D, Wang J Y, Zhang H J, Hu X B, Burns P, A Piper J, Piper J A 2002 Chem. Phys. Lett. 361 493

    [5]

    Lebedev V A, Voroshilov I V, Ignatiev B V, Gavrilenko A N, Isaev V A, Shestakov A V 2001 J. Lumin 92 139

    [6]

    Li P X, Zou S Z, Zhang X X, Li G 2010 Chin. Phys. B 19 074211

    [7]

    Wang S M, Du S F, Lu J, Zhang D X, Feng B H 2007 Chin. Phys. Soc. 1786-04

    [8]

    Kong L J, Xiao X S, Yang C X 2010 Chin. Phys. B 19 074212

    [9]

    Siebold M, Bock S, Schramm U, Xu B, Doualan J L, Camy P, Moncorgé R 2009 Appl. Phys. B 97 327

    [10]

    Ricaud S, Papadopoulos D N, Pellegrina A, Balembois F, Georges P, Courjaud A, Camy P, Doualan J L, Moncorgé R, Druon F 2011 Opt. Lett. 36 1602

    [11]

    Lucca A, Debourg G, Jacquemet M, Druon F, Balembois F, Georges P, Camy P, Doualan J L, Moncorgé R 2004 Opt. Lett. 29 2767

    [12]

    Ricaud S, Papadopoulos D N, Camy P, Doualan J L, Moncorgé R, Courjaud A, Mottay E, Georges P, Druon F 2010 Opt. Lett. 35 3757

    [13]

    Ricaud S, Druon F, Papadopoulos D N, Camy P, Doualan J L, Moncorgé R, Delaigue M, Zaouter Y, Courjaud A, Georges P, Mottay E 2010 Opt. Lett. 35 2415

    [14]

    Siebold M, Hein J, Kaluza M C, Uecker R 2007 Opt. Lett. 32 1818

    [15]

    Silva M A P, Messaddeq Y, Briois V, Poulain M, Villain F, Ribeiro S J L 2002 Solid State Ionics 147 135

    [16]

    Sorokin N I, Buchinskaya I I, Fedorov P P, Sobolev B P 2008 Inorg. Mater. 44 234

    [17]

    Karimov D N, Komar'kova O N, Sorokin N I, Bezhanov V A, Chernov S P, Popov P A, Sobolev B P 2010 Crystallogr. Rep. 55 518

    [18]

    Mouchovski J T, Temelkov K A, Vuchkov N K 2011 Prog. Cryst. Growth Charact Mater 57 1

    [19]

    Klimma D, Rabe M, Bertrama R, Uecker R, Parthier L 2008 J. Cryst. Growth 310 152

    [20]

    Basiev T T, Vasil'ev S V, Doroshenko M E, Konyushkin V A, Kuznetsov S V, Osiko V V, Fedorov P P 2007 Quant. Electron 37 934

    [21]

    Basiev T T, Doroshenko M, Fedorov P, Konyushkin V A, Kuznetsov S, Osiko V, Akchurin M 2008 Opt. Lett. 33 521

    [22]

    Basiev T T, Doroshenko M, Konyushkin V A 2011 Advances in Optical Materials (AIOM) paper: AIThA3

    [23]

    Youngmen R E, Smith C M 2008 Phys. Rev. B 78 014112

    [24]

    Fedorov P P, Osiko V V, Basiev T T, Orlovskii Yu V, Dukel'skii K V, Mironov I A, Demidenko V A, Smirnov A N 2007 Nanotechnologies in Russia 2 95

    [25]

    Siebold M, Bock S, Schramm U, Xu B, Doualan J L, Camy P, Moncorgé R 2009 Appl. Phys. B 97 327

    [26]

    Alimov O K, Basiev T T, Doroshenko M E, Fedorov P P, Konyushkin V A, Kouznetsov S V, Nakladov A N, Osiko V V, Jelinkova H, Šulc J 2009 Advanced Solid-State Photonics, OSA Technical Digest Series (CD) (Optical Society of America). paper WB25

    [27]

    Zeng X H, Zhao G J, Xu X D, Li H J, Xu J, Zhao Z W, He X M, Pang H Y, Jie M Y, Yan C F 2005 J. Cryst. Growth 274 106

    [28]

    Yu Y G, Wang J Y, Zhang H J, Wang Z P, Yu H H, Sun S Q, Xia H R, Jiang M H 2009 Opt. Express 17 9270

    [29]

    Ge W, Zhang H, Wang J, Liu J, Xu X, Hu X, Jiang M 2005 J. Appl. Phys. 98 013542

  • 引用本文:
    Citation:
计量
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出版历程
  • 收稿日期:  2011-10-20
  • 修回日期:  2011-12-23
  • 刊出日期:  2012-09-05

Yb:CaF2-SrF2激光晶体光谱性能以及热学性能的研究

  • 1. 宁波大学材料科学与化学工程学院, 宁波 315211;
  • 2. 中国科学院上海硅酸盐研究所, 上海 201800
    基金项目: 

    国家自然科学基金(批准号: 60938001, 60908030, 61178056)资助的课题.

摘要: 采用坩埚下降法生长了Yb: CaF2-SrF2晶体,测试了该晶体的吸收和荧光光谱 以及在不同温度下晶体的热扩散系数和热膨胀系数,并且计算了晶体的热膨胀系数以及在常温下的热导率. 采用对比的方法,对晶体的吸收光谱,荧光光谱,热学性能进行了分析.从吸收和荧光光谱结果表明: 在掺杂相对较高浓度的SrF2的混晶中, Yb3+吸收截面和发射截面比较大. Yb: CaF2-SrF2 (19%)晶体在1040 nm附近的发射截面比较大,光谱也比较宽. 这说明在掺杂相同浓度Yb时,混晶中CaF2, SrF2的比例不同,晶体的光谱性质不同, 主要原因是在混晶中晶体的无序度不同,晶体对称性降低,形成低对称光学中心. 从热扩散系数计算的热导率结果看出晶体具有比较好的热导率.

English Abstract

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