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基于磁过滤技术TiAlCN/TiAlN/TiAl复合体系腐蚀及摩擦学性能

陈淑年 廖斌 陈琳 张志强 沈永青 王浩琦 庞盼 吴先映 华青松 何光宇

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基于磁过滤技术TiAlCN/TiAlN/TiAl复合体系腐蚀及摩擦学性能

陈淑年, 廖斌, 陈琳, 张志强, 沈永青, 王浩琦, 庞盼, 吴先映, 华青松, 何光宇

Corrosion and tribological properties of TiAlCN/TiAlN/TiAlcomposite system deposited by magneticfliter cathode vacuum arctechnique

Chen Shu-Nian, Liao Bin, Chen Lin, Zhang Zhi-Qiang, Shen Yong-Qing, Wang Hao-Qi, Pang Pan, Wu Xian-Ying, Hua Qing-Song, He Guang-Yu
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  • 本文基于新型的磁过滤沉积技术(FCVA)研究了TiAlCN/TiAlN/TiAl多元复合涂层结构及不同C含量对其防腐耐磨性能的影响. 同时使用SEM, XRD, XPS, 电化学测试和摩擦磨损设备对其宏/微观性能进行了系统表征. 实验结果表明: 随C含量增加, C元素的存在形式从TiAlCN固溶相转化为TiAlCN固溶/非晶碳共存. 典型的TiAlCN固溶/非晶碳纳米复合结构TiAlCN/TiAlN/TiAl涂层不仅具有超高硬度和高韧性, 而且涂层中均匀无特征结构的非晶碳具有优异的自润滑效果, 通过结合各层的优势, 该结构涂层在3.5%NaCl电化学腐蚀试验中, Ecorr提高了5.6倍, 为0.271V, Icorr降低为原来的1/52, 为8.092 × 10–9 A·cm–2; 在干摩擦实验中, 摩擦系数降低了1/3, 为0.43, 磨损率降低了1/1.4, 为1.13 × 10–5 mm3·N–1·m–1.
    The experiment is based on novel magnetic filtered cathodic vacuum arc (FCVA) technology, the effects of the structure and C contents of TiAlCN/TiAlN/TiAl composite coating on anticorrosion and wear resistance were studied. The macro/micro properties of the coatings were systematically characterized by SEM, XRD, XPS, electrochemical tests and friction equipment. The results show that, with the increase of C content,the form of C element in the coatings transforms from the TiAlCN solid solution to the coexistence of crystallized TiAlCN/amorphous carbon. The TiAlCN/TiAlN/TiAl coating with TiAlCNcrystallized/amorphous carbon nanocomposite structure demonstrated excellent performanceby combining the advantages of each layer, which the hardness reaches an ultrahigh leveland the amorphous carbonwith excellent self-lubricating effect exists in the coating structure. In 3.5% NaCl electrochemical corrosion test, Ecorr increased by 5.6 times to 0.271 V, Icorr decreased by 1/52 to 8.092 ×10–9 A·cm–2. During the dry sliding, friction coefficient decreased by 1/3 to 0.43, and wear rate decreased by 1/1.4 to 1.13×10–5 mm3·N–1·m–1.
      通信作者: 廖斌, liaobingz@bnu.edu.cn
    • 基金项目: 国家级-国家科技重点实验室基金(614220207011802)
      Corresponding author: Liao Bin, liaobingz@bnu.edu.cn
    [1]

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    [2]

    PalDey S, Deevi S C 2003 Sci. Eng. A 342 58Google Scholar

    [3]

    Hsu C H, Lee C Y, Lee C C 2009 Thin Solid Films 17 5212

    [4]

    Brogren M, Harding G L, Karmhag R, Ribbing C G, Niklasson G A, Stenmark L 2000 Thin Solid Films 370 268Google Scholar

    [5]

    Hovsepian PEh, Münz W D, Medlock A, Gregory G 2000 Surf. Coat. Technol. 133–134 508

    [6]

    Warcholinski B, Gilewicz A 2011 Wear 271 2812Google Scholar

    [7]

    Zheng J Y, Hao J Y, Li u X, Gong Q Y, Liu W M 2012 Surf. Coat. Technol. 209 110Google Scholar

    [8]

    Agudelo L C, Ospina R, Castillo H A, Devia A 2008 Phys. Scr. T131 014006Google Scholar

    [9]

    Kamath G, Ehiasarian A P, Purandare Y, Hovsepian PEh 2011 Surf. Coat. Technol. 205 2823Google Scholar

    [10]

    Hovsepian PEh, Ehiasarian A P, Deeming A, Schimpf C 2008 Vacuum 82 1312Google Scholar

    [11]

    Yang L J, Zhang Z H, Dang X A, Li L 2014 Mater. Sci. Forum 789 449Google Scholar

    [12]

    AL-Bukhaiti M A, Al-hatab K A, Tillmann W, Hoffmann F, Sprute T 2014 Appl. Surf. Sci. 318 180Google Scholar

    [13]

    Kawata K, Sugimura H, Takai O 2001 Thin Solid Films 390 64Google Scholar

    [14]

    单磊, 王永欣, 李金龙 2013 中国表面工程 26 86Google Scholar

    Shan L, Wang Y X, Li J L 2013 China Surface Engineering 26 86Google Scholar

    [15]

    Kuptsov K A, Kiryukhantsev-Korneev P V, Sheveryko A N, ShtanskyDV 2013 Surf. Coat. Technol. 216 273Google Scholar

    [16]

    李刘合, 张海泉, 崔旭明 2001 物理学报 08 1549Google Scholar

    Li L H, Zhang H Q, Cui X M 2001 Acta Phys. Sin. 08 1549Google Scholar

    [17]

    Ferrari A C, Kleinsorge B, Morrison N A, Hart A 1999 J. Appl. Phys. 857 191

    [18]

    Zhang X H, Jiang J Q, Zeng Y Q, Lin J L, Wang F L, Moore J J 2008 Surf. Coat. Technol. 203 594Google Scholar

    [19]

    Zeng Y Q, Qiu Y D, Mao X Y, Tan X Y, Tan Z, Zhang X H, Chen J, Jiang J Q 2015 Thin Solid Films 584 283Google Scholar

    [20]

    Dreiling I, Stiens D, Chasse T 2010 Surf. Coat. Technol. 205 1339Google Scholar

    [21]

    Rodríguez R J, García J A, Medrano A, Rico M, Sánchez R, Martínez R, Labrugère C, Lahaye M, Guette A 2002 Vacuum 67 559Google Scholar

    [22]

    段晋辉, 梁银, 裴旺, 杨喜昆 2016 金属热处理 41 139

    Du J H, Liang Y, Pei W, Yang X K 2016 Heat Treatment of Metals 41 139

    [23]

    Jang C S, Jeon J H, Song P K, Kang M C, Kim K H 2005 Surf. Coat. Technol. 200 1501Google Scholar

    [24]

    Zehnder T, Schwaller P, Munnik F, Mikhailov S, Patscheider J 2004 J. Appl. Phys 95 4327Google Scholar

    [25]

    Matthews A, Franklin S, Holmberg K 2007 J. Phys. D: Appl. Phys. 40 5463Google Scholar

    [26]

    Musil J, Jirout M 2007 Surf. Coat. Technol. 201 5148Google Scholar

    [27]

    Massiani Y, Medjahed A, Crousier J P, Gravier P, Rebatel I 1991 Surf. Coat. Technol. 45 115Google Scholar

    [28]

    陈淑年, 廖斌, 吴先映, 陈琳, 黄杰, 何光宇 2019 中国表面工程 3 49Google Scholar

    Chen S N, Liao B, Wu X Y, Chen L, Huang J, He G Y 2019 China Surface Engineering 3 49Google Scholar

    [29]

    Vacandio F, Massiani Y, Gravier P, Rossi S, Bonora P L, Fedrizzi L 2001 Electrochim. Acta 46 3827Google Scholar

    [30]

    郑建云, 郝俊英, 刘小强, 龚秋雨, 刘维民 2013 摩擦学学报 33 87

    Zheng J Y, Hao J Y, Liu X Q, Gong Q Y, Liu W M 2013 Tribology 33 87

    [31]

    Eriksson A O, Ghafoor N, Jensen J, Näslund L Å, Johansson M P, Sjölen J, Odén M, Hultman L, Rosen J 2012 Surf. Coat. Technol. 213 145Google Scholar

    [32]

    Chen L, Yang B, Xu Y X, Pei F, Zhou L C, Du Y 2014 Thin Solid Films 556369

    [33]

    HoörlingA, Hultman L, Odén M, Sjölén J, Karlsson L 2002 J. Vac. Sci. Technol. A 20 1815

    [34]

    Cheng H H, Lee C Y, Lee C C 2009 ThinSolid Films 517 5212Google Scholar

    [35]

    Xie Z W, Wang L P, Wang X F, Huang L, Lu Y, Yan J C 2011 Trans. Nonferrous Met. Soc. China 21 470Google Scholar

    [36]

    Sampath Kumar T, Balasivanandha Prabu S, Manivasagam G 2014 J. Mater. Eng. Perform 23 2877Google Scholar

    [37]

    王泓 2002 博士学位论文 (西安: 西北工业大学)

    Wang H 2002 Ph. D. Dissertation (Xian: Northwestern Polytechnical University) (in Chinese)

  • 图 1  FCVA沉积装置示意图

    Fig. 1.  The schematic diagram of the FCVA deposition system.

    图 2  涂层中各层分布

    Fig. 2.  Distribution of the layers in the coating.

    图 3  不同C2H2流量沉积的TiAlCN/TiAlN/TiAl涂层的截面形貌 (a) 0 sccm; (b) 10 sccm; (c) 15 sccm

    Fig. 3.  Thecrosssection of TiAlCN/TiAlN/TiAl coatings deposited at various C2H2:(a) 0 sccm; (b) 10 sccm; (c) 15 sccm

    图 4  不同C2H2流量沉积的TiAlCN/TiAlN/TiAl涂层的XRD图谱

    Fig. 4.  XRD diffractogram of TiAlCN/TiAlN/TiAl coatings deposited at various C2H2.

    图 5  不同C2H2流量沉积的TiAlCN/TiAlN/TiAl涂层的拉曼谱图

    Fig. 5.  Raman spectra of TiAlCN/TiAlN/TiAl coatings deposited at various C2H2.

    图 6  S3(15 sccm, 12.39 at.%C)的XPS图谱 (a) N 1s; (b) C 1s; (c) Ti 2p; (d) Al 2p

    Fig. 6.  XPS analysis of S3: (a) N 1s;(b) C 1s;(c) Ti 2p; (d) Al 2p.

    图 7  不同C2H2流量沉积的TiAlCN/TiAlN/TiAl涂层在3.5 wt-% NaCl溶液中的动电位极化曲线

    Fig. 7.  Potentiodynamic polarization curves of TiAlCN/TiAlN/TiAl coatings in 3.5 wt-% NaCl solution.

    图 8  不同C2H2流量沉积的TiAlCN/TiAlN/TiAl涂层电化学腐蚀的数据结果

    Fig. 8.  Results of Electrochemical corrosion characterization activities for TiAlCN/TiAlN/TiAl coatings deposited at various C2H2.

    图 9  不同C2H2流量沉积的TiAlCN/TiAlN/TiAl涂层电化学阻抗谱

    Fig. 9.  Electrochemical impedance spectroscopy of TiAlCN/TiAlN/TiAl coatings deposited at various C2H2.

    图 10  不同C2H2流量沉积的TiAlCN/TiAlN/TiAl涂层的阻抗-频率图

    Fig. 10.  Bode plots ofTiAlCN/TiAlN/TiAl coatings deposited at various C2H2.

    图 11  不同C2H2流量沉积的TiAlCN/TiAlN/TiAl涂层的相角-频率图

    Fig. 11.  Bode phase angle plots ofTiAlCN/TiAlN/TiAl coatings deposited at various C2H2.

    图 12  不同C2H2流量沉积的TiAlCN/TiAlN/TiAl涂层表面SEM形貌(a)0 sccm; (b)10 sccm; (c)15 sccm

    Fig. 12.  SEM surface micrographs of TiAlCN/TiAlN/TiAl coatings deposited at various C2H2: (a)0 sccm; (b)10 sccm; (c)15 sccm.

    图 13  不同C2H2流量沉积的TiAlCN/TiAlN/TiAl涂层的摩擦系数

    Fig. 13.  Friction coefficient curves of TiAlCN/TiAlN/TiAl coatings deposited at various C2H2.

    图 14  不同C2H2流量沉积的TiAlCN/TiAlN/TiAl涂层的摩擦系数和磨损率

    Fig. 14.  Friction coefficientand wear rate of TiAlCN/TiAlN/TiAl coatings deposited at various C2H2.

    图 15  不同C2H2流量沉积的TiAlCN/TiAlN/TiAl涂层磨痕区的SEM图像和EDS能谱分析 (a), (b) 0 sccm; (c), (d) 10 sccm; (e), (f) 15 sccm

    Fig. 15.  SEM micrographs of the wear track and EDS results of TiAlCN/TiAlN/TiAl coatings deposited at various C2H2: (a), (b) 0 sccm; (c), (d) 10 sccm; (e), (f) 15 sccm.

    图 16  不同C2H2流量沉积的TiAlCN/TiAlN/TiAl涂层磨痕处的拉曼谱图

    Fig. 16.  Raman spectra of wear track of TiAlCN/TiAlN/TiAl coatings deposited at various C2H2.

    表 1  不同C2H2流量沉积的TiAlCN/TiAlN/TiAl涂层的元素相对含量

    Table 1.  Chemical composition of TiAlCN/TiAlN/TiAl coatings deposited at various C2H2.

    SampleC2H2/sccmTi/at.%Al/at.%N/at.%C/at.%
    TiAlN/TiAlS1030.8722.8546.28
    TiAlCN/TiAlN/TiAlS21028.6421.5241.238.61
    TiAlCN/TiAlN/TiAlS31527.6022.9537.0712.39
    下载: 导出CSV

    表 2  不同C2H2流量沉积的TiAlCN/TiAlN/TiAl涂层的显微硬度、杨氏模量和H/E比值

    Table 2.  Microhardness、Modules and ratio of H/E of TiAlCN/TiAlN/TiAl coatings deposited at various C2H2.

    SampleC2H2/sccmE/GPaH/GPaH/E
    TiAlN/TiAlS10290.2030.530.105
    TiAlCN/TiAlN/TiAlS210310.6541.160.133
    TiAlCN/TiAlN/TiAlS315316.1444.360.140
    下载: 导出CSV
  • [1]

    王均涛, 刘平, 李伟, 郑康培 2010 热加工工艺 20 104Google Scholar

    Wang J T, Liu P, Li W, Zheng K P 2010 Hot Working Technology 20 104Google Scholar

    [2]

    PalDey S, Deevi S C 2003 Sci. Eng. A 342 58Google Scholar

    [3]

    Hsu C H, Lee C Y, Lee C C 2009 Thin Solid Films 17 5212

    [4]

    Brogren M, Harding G L, Karmhag R, Ribbing C G, Niklasson G A, Stenmark L 2000 Thin Solid Films 370 268Google Scholar

    [5]

    Hovsepian PEh, Münz W D, Medlock A, Gregory G 2000 Surf. Coat. Technol. 133–134 508

    [6]

    Warcholinski B, Gilewicz A 2011 Wear 271 2812Google Scholar

    [7]

    Zheng J Y, Hao J Y, Li u X, Gong Q Y, Liu W M 2012 Surf. Coat. Technol. 209 110Google Scholar

    [8]

    Agudelo L C, Ospina R, Castillo H A, Devia A 2008 Phys. Scr. T131 014006Google Scholar

    [9]

    Kamath G, Ehiasarian A P, Purandare Y, Hovsepian PEh 2011 Surf. Coat. Technol. 205 2823Google Scholar

    [10]

    Hovsepian PEh, Ehiasarian A P, Deeming A, Schimpf C 2008 Vacuum 82 1312Google Scholar

    [11]

    Yang L J, Zhang Z H, Dang X A, Li L 2014 Mater. Sci. Forum 789 449Google Scholar

    [12]

    AL-Bukhaiti M A, Al-hatab K A, Tillmann W, Hoffmann F, Sprute T 2014 Appl. Surf. Sci. 318 180Google Scholar

    [13]

    Kawata K, Sugimura H, Takai O 2001 Thin Solid Films 390 64Google Scholar

    [14]

    单磊, 王永欣, 李金龙 2013 中国表面工程 26 86Google Scholar

    Shan L, Wang Y X, Li J L 2013 China Surface Engineering 26 86Google Scholar

    [15]

    Kuptsov K A, Kiryukhantsev-Korneev P V, Sheveryko A N, ShtanskyDV 2013 Surf. Coat. Technol. 216 273Google Scholar

    [16]

    李刘合, 张海泉, 崔旭明 2001 物理学报 08 1549Google Scholar

    Li L H, Zhang H Q, Cui X M 2001 Acta Phys. Sin. 08 1549Google Scholar

    [17]

    Ferrari A C, Kleinsorge B, Morrison N A, Hart A 1999 J. Appl. Phys. 857 191

    [18]

    Zhang X H, Jiang J Q, Zeng Y Q, Lin J L, Wang F L, Moore J J 2008 Surf. Coat. Technol. 203 594Google Scholar

    [19]

    Zeng Y Q, Qiu Y D, Mao X Y, Tan X Y, Tan Z, Zhang X H, Chen J, Jiang J Q 2015 Thin Solid Films 584 283Google Scholar

    [20]

    Dreiling I, Stiens D, Chasse T 2010 Surf. Coat. Technol. 205 1339Google Scholar

    [21]

    Rodríguez R J, García J A, Medrano A, Rico M, Sánchez R, Martínez R, Labrugère C, Lahaye M, Guette A 2002 Vacuum 67 559Google Scholar

    [22]

    段晋辉, 梁银, 裴旺, 杨喜昆 2016 金属热处理 41 139

    Du J H, Liang Y, Pei W, Yang X K 2016 Heat Treatment of Metals 41 139

    [23]

    Jang C S, Jeon J H, Song P K, Kang M C, Kim K H 2005 Surf. Coat. Technol. 200 1501Google Scholar

    [24]

    Zehnder T, Schwaller P, Munnik F, Mikhailov S, Patscheider J 2004 J. Appl. Phys 95 4327Google Scholar

    [25]

    Matthews A, Franklin S, Holmberg K 2007 J. Phys. D: Appl. Phys. 40 5463Google Scholar

    [26]

    Musil J, Jirout M 2007 Surf. Coat. Technol. 201 5148Google Scholar

    [27]

    Massiani Y, Medjahed A, Crousier J P, Gravier P, Rebatel I 1991 Surf. Coat. Technol. 45 115Google Scholar

    [28]

    陈淑年, 廖斌, 吴先映, 陈琳, 黄杰, 何光宇 2019 中国表面工程 3 49Google Scholar

    Chen S N, Liao B, Wu X Y, Chen L, Huang J, He G Y 2019 China Surface Engineering 3 49Google Scholar

    [29]

    Vacandio F, Massiani Y, Gravier P, Rossi S, Bonora P L, Fedrizzi L 2001 Electrochim. Acta 46 3827Google Scholar

    [30]

    郑建云, 郝俊英, 刘小强, 龚秋雨, 刘维民 2013 摩擦学学报 33 87

    Zheng J Y, Hao J Y, Liu X Q, Gong Q Y, Liu W M 2013 Tribology 33 87

    [31]

    Eriksson A O, Ghafoor N, Jensen J, Näslund L Å, Johansson M P, Sjölen J, Odén M, Hultman L, Rosen J 2012 Surf. Coat. Technol. 213 145Google Scholar

    [32]

    Chen L, Yang B, Xu Y X, Pei F, Zhou L C, Du Y 2014 Thin Solid Films 556369

    [33]

    HoörlingA, Hultman L, Odén M, Sjölén J, Karlsson L 2002 J. Vac. Sci. Technol. A 20 1815

    [34]

    Cheng H H, Lee C Y, Lee C C 2009 ThinSolid Films 517 5212Google Scholar

    [35]

    Xie Z W, Wang L P, Wang X F, Huang L, Lu Y, Yan J C 2011 Trans. Nonferrous Met. Soc. China 21 470Google Scholar

    [36]

    Sampath Kumar T, Balasivanandha Prabu S, Manivasagam G 2014 J. Mater. Eng. Perform 23 2877Google Scholar

    [37]

    王泓 2002 博士学位论文 (西安: 西北工业大学)

    Wang H 2002 Ph. D. Dissertation (Xian: Northwestern Polytechnical University) (in Chinese)

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出版历程
  • 收稿日期:  2020-01-03
  • 修回日期:  2020-03-23
  • 刊出日期:  2020-05-20

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