Recent progress in aqueous akali-metal-ion batteries at low temperatures

Han Shuai; Guo Qiu-Bo; Lu Ya-Xiang; Chen Li-Quan; Hu Yong-Sheng

doi:10.7498/aps.72.20230024

Abstract

Aqueous alkali-metal-ion batteries are a popular frontier research area, expected to apply for large-scale energy storage due to their high safety, low cost, and environmental friendliness. Depending on diversified social development, batteries ought to function in various ambient, including polar regions and high-altitude locales. Delivering excellent electrochemical performance at low temperatures is crucial to develop aqueous alkali-metal-ion batteries. This review summarizes the representative research progress in the field of aqueous low-temperature alkali-metal-ion batteries in recent years, based on the subjects of electrolyte, electrode, and interface. Firstly, we discussed the challenges of aqueous alkali-metal-ion batteries operated at low temperatures and the corresponding failure mechanisms. At subzero temperatures, aqueous alkali-metal-ion batteries couldn't work or exhibit little capacity, arising from the frozen electrolytes, electrode materials with slow kinetics, and huge interface impedances, which seriously limits their wide application in low-temperature conditions. Then, combined with the latest research work, various strategies have been investigated to improve the electrochemical performance of batteries at low temperatures. To date, the strategies for reducing the freezing point of electrolytes have primarily focused on breaking H-bonds between free water molecules by increasing salt concentration, adding organic/inorganic additives, and using hydrogel as electrolytes. In terms of electrodes, the related studies have concentrated on regulating the structure and morphology of electrodes, introducing the dual ion battery mechanism, and using organic materials and Zn electrodes to alleviate the slow ion dynamics of electrodes. In addition, adding appropriate organic solvents that can generate protective layers with low interface impedance on the electrode surface in the electrolyte can also improve the low-temperature performance of aqueous alkali-metal-ion batteries. Finally, we evaluated multi-dimensionally all strategies, expected to provide a comprehensive reference and point out the direction for the further improvement and practical application of the aqueous alkali-metal-ion batteries at low temperatures.

Keywords:

aqueous low-temperature alkali-metal-ion batteries /
electrolytes /
electrodes /
interface

Authors and contacts

1.
Institute of Physics, Chinese Academy of Sciences, Beijing 100190, China
2.
College of Materials Science and Optoelectronic Technology, University of Chinese Academy of Sciences, Beijing 100049, China
3.
Huairou Division, Institute of Physics, Chinese Academy of Sciences, Beijing 101400, China

Corresponding author: Lu Ya-Xiang, yxlu@iphy.ac.cn ; Hu Yong-Sheng, yshu@iphy.ac.cn

Funds: Project supported by the Natural Science Foundation of Beijing, China (Grant No. 2212022), the National Natural Science Foundation of China (Grant Nos. 51725206, 52122214, 52072403), Youth Innovation Promotion Association of the Chinese Academy of Sciences (Grant No. 2020006), and the Jiangsu Provincial Carbon Peak and Neutrality Innovation Program (Industry Tackling on Prospect and Key Technology), China (Grant No. BE2022002-5).

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References

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Cited By

图 1 (a) 近几年与低温水系碱金属离子电池相关的文章数量统计; (b) 水系碱金属离子电池的低温发展策略总结

Figure 1. (a) The number of articles related to aqueous alkali-metal-ion batteries at low temperatures in recent years; (b) the strategies for alkali metal-ions batteries at low temperatures.

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图 2 (a) 35 m LiFSI, 25 m LiFSI+10 m LiFTFSI, 25 m LiFSI+10 m LiTFSI的DSC曲线^[31]; (b) 25 m LiFSI+10 m LiFTFSI电解液和25 m LiFSI+10 m LiTFSI电解液在0 °C下保存4周后的照片^[31]; (c) LiPTFSI, LiOTf及其二元混合物的水溶液的相图^[32]; (d) 水/DMSO (χ_DMSO= 0.30)混合物的DSC曲线(在水溶液中加入摩尔分数为0.3的DMSO)^[15]; (e)—(g) 三种全电池在25和–50 ℃的充放电曲线^[15]; (h) Na₂CoFe(CN)₆//AC 全电池在25和–30 ℃下的充放电曲线^[36]; (i) LTP@C //PIL-OH 水凝胶//AC 全电池在不同温度下的充放电曲线^[18]; (j) 全电池连续在不同温度下循环的容量变化^[18]

Figure 2. (a) DSC curves of different electrolytes (35 m LiFSI, 25 m LiFSI+10 m LiFTFSI, 25 m LiFSI+10 m LiTFSI) between 60 and –120 ℃^[31]; (b) the optical photographs of 25 m LiFSI+10 m LiFTFSI and 25 m LiFSI+10 m LiTFSI after storage at 0 ℃ for 4 weeks^[31]; (c) the phase diagrams of aqueous solutions of LiPTFSI, LiOTf, and their binary mixtures^[32]; (d) the DSC result of χ_DMSO= 0.3 electrolyte solvent^[15]; (e)–(g) GCD curves of different batteries at 25 and –50 ℃^[15]; (h) the GCD curves of the Na₂CoFe(CN)₆//AC full cells at 25 and –30 ℃ for different cycles^[36]; (i) the GCD curves of LTP@C //PIL-OH hydrogel//AC full cells at different temperatures^[18]; (j) the capacity change for the full cells cycled at different temperatures continuously^[18]

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图 3 (a) α-V₂O₅和δ-K_0.5V₂O₅ (KVO) 两种电极的CV曲线^[20]; (b)—(d) δ-K_0.5V₂O₅ (KVO) 电极的三种可能的离子扩散路径示意图^[20]; (e)—(g) 三种路径对应的K⁺传输势垒^[20]; (h) α-V₂O₅和δ₀-V₂O₅ (KVO) 两种电极的电子结构^[20]; (i) 不同温度下的δ-K_0.5V₂O₅ (KVO)//PTCDI 软包全电池充放电曲线^[20]

Figure 3. (a) The CV curves of α-V₂O₅ and reconstructed δ-K_0.5V₂O₅ (KVO) electrodes^[20]; (b)–(d) the schematics of three possible pathways for K-ion diffusion^[20]; (e)–(g) the transport energy batteries of three kinds of K⁺ pathways^[20]; (h) the electronic structure results of α-V₂O₅ and δ₀-V₂O₅ (KVO) electrodes from DOS calculating^[20]; (i) the GCD curves of δ-K_0.5V₂O₅ (KVO)//PTCDI full batteries at different temperatures^[20].

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图 4 (a) PT电极的晶体结构^[13]; (b) PT电极在不同电流密度下的充放电曲线^[13]; (c) NiHCF//17 m NaClO₄//PT全电池在不同电流密度下的充放电曲线^[13]; (d) PANI//3 ZC6 LC//Zn全电池在–30和–50 ℃下的充放电曲线^[25]; (e) PANI//Zn全电池在–50 ℃下的循环性能^[25]

Figure 4. (a) The crystal structure of the PT electrode^[13]; (b) the GCD curves of PT electrode at different current densities^[13]; (c) the GCD curves of NiHCF//17 m NaClO₄//PT full cells at different current densities^[13]; (d) the GCD curves of PANI//3 ZC6 LC//Zn full cells at –30 and –50 ℃^[25]; (e) the cycle performance of PANI//Zn full cells at –50 ℃^[25].

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图 5 (a) Ni(OH)₂//2 m NaClO₄//NaTi₂(PO₄)₃(NTP@C)双离子电池机理示意图^[27]; (b) Ni(OH)₂//NaTi₂(PO₄)₃(NTP@C)全电池在不同电流密度下的充放电曲线^[27]; (c) Ni(OH)₂//NaTi₂(PO₄)₃(NTP@C)全电池在不同温度下的循环性能^[27]; (d) PC//1 m TPABr+9.1 m LiBr//NDPI全电池机理图^[26]; (e) PC电极在室温下的充放电曲线^[26]; (f) PC电极在低温下的倍率性能^[26]; (g) PC//1 m TPABr+9.1 m LiBr//NDPI全电池在不同温度下的充放电曲线^[26]; (h) PC//1 m TPABr+9.1 m LiBr//NDPI全电池的循环性能^[26]

Figure 5. (a) The schematic illustration of Ni(OH)₂//2 m NaClO₄//NaTi₂(PO₄)₃(NTP@C) full cell^[27]; (b) the GCD curves of Ni(OH)₂//NaTi₂(PO₄)₃(NTP@C) full cells at different current densities^[27]; (c) the cycle performances of Ni(OH)₂//NaTi₂(PO₄)₃(NTP@C) full cells at different temperatures^[27]; (d) the schematic illustration of PC//1 m TPABr+9.1 m LiBr//NDPI full cell^[26]; (e) the GCD curves of PC electrodes at room temperature^[26]; (f) the rate performances of PC electrodes from –60 to –20 ℃^[26]; (g) the GCD curves of PC//1 m TPABr+9.1 m LiBr//NDPI full cells at different temperatures^[26]; (h) the cycle performances of PC//1 m TPABr+9.1 m LiBr//NDPI full cells^[26].

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图 6 (a) LiCoO₂电极在不同电解液和不同温度下的循环性能^[38]; (b)—(d) 有机电解液和水系电解液的阻抗对比^[38]

Figure 6. (a) The cycle performances of LiCoO₂ electrodes in different states^[38]; (b)–(d) the impedances comparison between aqueous (sat. LiCl) and organic (1 M LiPF6 in 1:1 EC: DEC) electrolyte systems^[38].

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图 7 (a) LiMn₂O₄(LMO)//Li₄Ti₅O₁₂(LTO)全电池在BSiS-D0.28和BSiS-A0.5电解液中的电化学性能^[39]; (b)—(d) R_E, R_SEI和R_CT的阻抗拟合结果^[39]

Figure 7. (a) The cycle performances of LiMn₂O₄(LMO)//Li₄Ti₅O₁₂(LTO) full cells tested in different electrolytes^[39]; (b)–(d) fitting results of R_E, R_SEI, and R_CT obtained from EIS^[39].

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图 8 (a) Na₃V₂(PO₄)₃ //10 m NaClO₄–0.17 m Zn(CH₃COO)₂–2 wt% VC//Zn全电池的机理示意图^[28]; (b) 两种电解液的Na₃V₂(PO₄)₃//Zn全电池在–10 ℃下循环前后的阻抗结果^[28]; (c) Na₃V₂(PO₄)₃ //10 m NaClO₄-0.17 m Zn(CH₃COO)₂–2 wt% VC//Zn全电池低温下的倍率性能^[28]; (d) Na₃V₂(PO₄)₃ //10 m NaClO₄-0.17 m Zn(CH₃COO)₂-2 wt% VC//Zn全电池在–10 ℃的循环性能^[28]

Figure 8. (a) The schematic illustration of Na₃V₂(PO₄)₃ //10 m NaClO₄-0.17 m Zn(CH₃COO)₂-2 wt% VC//Zn full cell^[28]; (b) the EIS results of Na₃V₂(PO₄)₃//Zn full batteries before and after 30 cycles at –10 ℃ in the two electrolytes^[28]; (c) the rate performances of Na₃V₂(PO₄)₃ //10 m NaClO₄-0.17 m Zn(CH₃COO)₂-2 wt% VC//Zn full cells at low temperatures^[28]; (d) the cycle performances of Na₃V₂(PO₄)₃ //10 m NaClO₄-0.17 m Zn(CH₃COO)₂-2 wt% VC//Zn full cells at –10 ℃^[28].

DownLoad: Full-Size Img PowerPoint

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[2]	Larcher D, Tarascon J M 2015 Nat. Chem. 7 19 Google Scholar
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[7]	Suo L, Borodin O, Gao T, Olguin M, Ho J, Fan X, Luo C, Wang C, Xu K 2015 Science 350 938 Google Scholar
[8]	Yue J, Suo L 2021 Energy Fuels 35 9228 Google Scholar
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[14]	Zhu K J, Sun Z Q, Jin T, Chen X C, Si Y C, Li H X, Jiao L F 2022 Batteries Supercaps 5 202200308
[15]	Nian Q, Wang J, Liu S, Sun T, Zheng S, Zhang Y, Tao Z, Chen J 2019 Angew. Chem. Int. Ed. 58 16994 Google Scholar
[16]	Ma Z, Chen J, Vatamanu J, Borodin O, Bedrov D, Zhou X, Zhang W, Li W, Xu K, Xing L 2022 Energy Storage Materials 45 903
[17]	Liu T, Liu K-T, Wang J, Ji X, Lan P, Mu Z, Pan Y, Cheng S, Liu M 2021 Energy Storage Materials 41 133
[18]	Hu Y, Shi R W, Ren Y Y, Peng W S, Feng C D, Zhao Y, Zheng S J, Li W Z, Sun Z, Guo J N, Guo S Y, Wang X L, Yan F 2022 Adv. Funct. Mater. 32 2203081 Google Scholar
[19]	Tron A, Jeong S, Park Y D, Mun J 2019 ACS Sustainable Chem. Eng. 7 14531 Google Scholar
[20]	Liang G, Gan Z, Wang X, Jin X, Xiong B, Zhang X, Chen S, Wang Y, He H, Zhi C 2021 ACS Nano 15 17717 Google Scholar
[21]	Zhu K, Sun Z, Li Z, Liu P, Chen X, Jiao L 2022 Energy Storage Mater. 53 523 Google Scholar
[22]	Sun T, Liu C, Wang J, Nian Q, Feng Y, Zhang Y, Tao Z, Chen J 2020 Nano Res. 13 676 Google Scholar
[23]	Sun Y, Zhang Y, Xu Z, Gou W, Han X, Liu M, Li CM 2022 ChemSusChem 202201362
[24]	Zhu M, Wang X, Tang H, Wang J, Hao Q, Liu L, Li Y, Zhang K, Schmidt O G 2020 Adv. Funct. Mater. 30 1907218 Google Scholar
[25]	Yan C, Wang Y, Deng X, Xu Y 2022 Nano-Micro Lett. 14 98 Google Scholar
[26]	Wang M, Li T, Yin Y, Yan J, Zhang H, Li X 2022 Adv. Energy Mater. 12 2200728 Google Scholar
[27]	Nian Q, Liu S, Liu J, Zhang Q, Shi J, Liu C, Wang R, Tao Z, Chen J 2019 ACS Appl. Energy Mater. 2 4370 Google Scholar
[28]	Liu S, Lei T, Song Q, Zhu J, Zhu C 2022 ACS Appl. Mater. Interfaces 14 11425 Google Scholar
[29]	Pipolo S, Salanne M, Ferlat G, Klotz S, Saitta AM, Pietrucci F 2017 Phys. Rev. Lett. 119 245701 Google Scholar
[30]	Leadbetter A, Ward R, Clark J, Tucker P, Matsuo T, Suga H 1985 J. Chem. Phys. 82 424 Google Scholar
[31]	Reber D, Kühnel R S, Battaglia C 2019 ACS Mater. Lett. 1 44 Google Scholar
[32]	Becker M, Kühnel R S, Battaglia C 2019 ChemComm 55 12032 Google Scholar
[33]	Liu J, Yang C, Chi X, Wen B, Wang W, Liu Y 2022 Adv. Funct. Mater. 32 2106811 Google Scholar
[34]	Reber D, Borodin O, Becker M, Rentsch D, Thienenkamp J H, Grissa R, Zhao W, Aribia A, Brunklaus G, Battaglia C 2022 Adv. Funct. Mater. 32 2112138 Google Scholar
[35]	Bi H, Wang X, Liu H, He Y, Wang W, Deng W, Ma X, Wang Y, Rao W, Chai Y, Ma H, Li R, Chen J, Wang Y, Xue M 2020 Adv. Mater. 32 2000074 Google Scholar
[36]	Zhu K, Li Z, Sun Z, Liu P, Jin T, Chen X, Li H, Lu W, Jiao L 2022 Small 18 2107662 Google Scholar
[37]	Ao H, Zhao Y, Zhou J, Cai W, Zhang X, Zhu Y, Qian Y 2019 J. Mater. Chem. A 7 18708 Google Scholar
[38]	Ramanujapuram A, Yushin G 2018 Adv. Energy Mater. 8 1802624 Google Scholar
[39]	Chen J, Vatamanu J, Xing L, Borodin O, Chen H, Guan X, Liu X, Xu K, Li W 2020 Adv. Energy Mater. 10 1902654 Google Scholar
[40]	Liu T, Zhang M, Wang Y L, Wang Q Y, Lü C, Liu K X, Suresh S, Yin Y H, Hu Y Y, Li Y S, Liu X B, Zhong X W, Xia B Y, Wu Z P 2018 Adv. Energy Mater. 8 1802349 Google Scholar
[41]	Lee J, Lee C L, Park K, Kim I D 2014 J. Power Sources 248 1211 Google Scholar
[42]	Madzvamuse A, Hamenu L, Mohammed L, Ko JM 2018 ChemistrySelect 3 10805 Google Scholar

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Vol. 72, Issue 7 - 2023-04-05

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