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Bulk titanium borides (TiB2) have been successfully synthesized from the stoichiometric boron and titanium powders at high pressure and high temperature (HPHT). The density of TiB2 is higher than 99%. The Vicker's hardness of TiB2 as synthesized is 39.6 GPa which is near to result of the supehard materials. While TiB2 show good metallic characters with the resistivity, 10-8 Ωm, which is near to the value of the single crystal of TiB2. The enhanced properties of TiB2 as synthesized may be attributed to the higher density and uniform crystal size.
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Keywords:
- titanium borides /
- high pressure and high temperature /
- vicker'
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[2] Gao Q F, G鹡ter K, Walter S 2008 Adv. Mater. 20 3620
[3] Chung H Y, Michelle B W, Jonathan B L, Abby K 2007 Science. 318 316
[4] Liang Y C, Guo W L, Fang Z 2007 Acta. Phys. Sin. 56 4847 (in Chinese) [梁拥成, 郭万林, 方忠 2007 物理学报 56 4847]
[5] Reza M, Andrew T L, Miao X 2011 PNAS 27 10958
[6] Subramanian C 2007 International Journal of Refractory Metals & Hard Materials 25 345
[7] June H P, Yong H L, Young H K, Hyoun E K 2000 J. Am. Ceram. Soc. 83 1542
[8] Vis R K, Mannan S K, Kumar K S, Wolf A 1989 J. Mater. Sci. Lett. 8 409
[9] Xiang J, Li L P, Su W H 2003 Acta. Phys. Sin. 52 1474 (in Chinese) [向军, 李莉萍, 苏文辉 2003 物理学报 52 1474]
[10] Haimin D, Xiangfa L, Jinfeng N 2012 Materials Characterization 63 56
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[13] Lepakova O K., Raskolenko L G, Maksimov Y M 2000 Inorganic Materials 36690
[14] He P, Wang W M 2006 Rare Metals Letters 25(1) (in Chinese) [何平, 王为民 2006 稀有金属快报 25(1)]
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[16] Cheng J Y, Zheng H F, Zeng Y C 2000 Science & Technology Review 6 13 (in Chinese) [陈晋阳, 郑海飞, 曾贻善 2000 科技导报 613]
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[18] Kumar T S, Kumar A, James A R, Pamu D 2012 Journal of the Australian Ceramic Society Volume 48 96
[19] Dai S S 1984 Reliability Test and Statistical Analysis (Vol. 2) (National Defence Industry Press) p504 (in Chinese) [戴树森 1984 可靠性试验及其统计分析(下)(国防工业出版社) 第507页]
[20] Cheng G L, Peng Z Z, Fan S G, Liu Y C 2010 Bull. Chin. Ceram. Soc. 2 29 (in Chinese) [陈广乐, 彭珍珍, 范仕刚, 刘允超2010硅酸盐通报 2 29]
[21] Park J H, Lee Y H, Koh Y H, Kim H E 2000 Communications of the American Ceramic Society 83 1542
[22] Kunca F, Musila J, Mayrhoferb P H, Mittererb C 2003 Surface and Coatings Technology 53 174
[23] Yu Y L 2000 Principles of Metallography (Metallurgical Industry Press) p321-425 (in Chinese) [余永宁 2000 金属学原理(冶金工业出版社) 第321–425页]
[24] Ohfuji H, Okimoto S, Kunimoto T, Isobe F 2012 Phys. Chem. Minerals. 39 543
[25] Li X Y, Manghnani M H, Li C M 1996 J. Appl. Phys. 80 7
[26] Ra M , Wang C C, Chen W, S A Akbar 1995 J. Am. Ceram. Soc. 78 1380
[27] Mcleod A D, Haggerty J S, Sadoway D R 1984 J. Am. Ceram. Soc. 67 705
[28] Konigshofer R, Fu S, Lengauer W, Haas R, Rabitsch K 2005 International Journal of Refractory Metals & Hard Materials 23 50
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[1] Wang M, Li Y W, Cui T, Ma Y M, Zou G T 2008 Appl. Phys. Lett. 93 101905
[2] Gao Q F, G鹡ter K, Walter S 2008 Adv. Mater. 20 3620
[3] Chung H Y, Michelle B W, Jonathan B L, Abby K 2007 Science. 318 316
[4] Liang Y C, Guo W L, Fang Z 2007 Acta. Phys. Sin. 56 4847 (in Chinese) [梁拥成, 郭万林, 方忠 2007 物理学报 56 4847]
[5] Reza M, Andrew T L, Miao X 2011 PNAS 27 10958
[6] Subramanian C 2007 International Journal of Refractory Metals & Hard Materials 25 345
[7] June H P, Yong H L, Young H K, Hyoun E K 2000 J. Am. Ceram. Soc. 83 1542
[8] Vis R K, Mannan S K, Kumar K S, Wolf A 1989 J. Mater. Sci. Lett. 8 409
[9] Xiang J, Li L P, Su W H 2003 Acta. Phys. Sin. 52 1474 (in Chinese) [向军, 李莉萍, 苏文辉 2003 物理学报 52 1474]
[10] Haimin D, Xiangfa L, Jinfeng N 2012 Materials Characterization 63 56
[11] Kunal K, Ramachandran R, Norman M W 2011 J. Eng. Mat. and Tec. 133 024501-1
[12] Roy S K, Biswas A, Banerjee S 1993 Mater. Sci. 5 347
[13] Lepakova O K., Raskolenko L G, Maksimov Y M 2000 Inorganic Materials 36690
[14] He P, Wang W M 2006 Rare Metals Letters 25(1) (in Chinese) [何平, 王为民 2006 稀有金属快报 25(1)]
[15] Xi S T G 1990 Powder metallurgy 37(5) 898 (in Chinese) [西山腾广 1990 粉体粉末冶金 37(5) 898]
[16] Cheng J Y, Zheng H F, Zeng Y C 2000 Science & Technology Review 6 13 (in Chinese) [陈晋阳, 郑海飞, 曾贻善 2000 科技导报 613]
[17] Wang F L, He D W, Fang L M, Chen X F, Li Y J, Zhang W, Zhang J, Kou Z L, Peng F 2008 Acta Phys. Sin. 57 5429 (in Chinese) [王福龙, 贺端威, 房雷鸣, 陈晓芳, 李拥军, 张伟, 张剑, 寇自力, 彭放 2008 物理学报 57 5429]
[18] Kumar T S, Kumar A, James A R, Pamu D 2012 Journal of the Australian Ceramic Society Volume 48 96
[19] Dai S S 1984 Reliability Test and Statistical Analysis (Vol. 2) (National Defence Industry Press) p504 (in Chinese) [戴树森 1984 可靠性试验及其统计分析(下)(国防工业出版社) 第507页]
[20] Cheng G L, Peng Z Z, Fan S G, Liu Y C 2010 Bull. Chin. Ceram. Soc. 2 29 (in Chinese) [陈广乐, 彭珍珍, 范仕刚, 刘允超2010硅酸盐通报 2 29]
[21] Park J H, Lee Y H, Koh Y H, Kim H E 2000 Communications of the American Ceramic Society 83 1542
[22] Kunca F, Musila J, Mayrhoferb P H, Mittererb C 2003 Surface and Coatings Technology 53 174
[23] Yu Y L 2000 Principles of Metallography (Metallurgical Industry Press) p321-425 (in Chinese) [余永宁 2000 金属学原理(冶金工业出版社) 第321–425页]
[24] Ohfuji H, Okimoto S, Kunimoto T, Isobe F 2012 Phys. Chem. Minerals. 39 543
[25] Li X Y, Manghnani M H, Li C M 1996 J. Appl. Phys. 80 7
[26] Ra M , Wang C C, Chen W, S A Akbar 1995 J. Am. Ceram. Soc. 78 1380
[27] Mcleod A D, Haggerty J S, Sadoway D R 1984 J. Am. Ceram. Soc. 67 705
[28] Konigshofer R, Fu S, Lengauer W, Haas R, Rabitsch K 2005 International Journal of Refractory Metals & Hard Materials 23 50
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